1-(2',6'-dimethylphenyl)-2-propanone

Base Information

• Chemical Name: 1-(2',6'-dimethylphenyl)-2-propanone
• CAS No.: 205826-75-1
• Molecular Formula: C₁₁H₁₄O
• Molecular Weight: 162.232

Synonyms:

Chemical Property of 1-(2',6'-dimethylphenyl)-2-propanone

Chemical Property:

Purity/Quality:

(2,6-Dimethylphenyl)acetone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2',6'-dimethylphenyl)-2-propanone

There total 3 articles about 1-(2',6'-dimethylphenyl)-2-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

→ 1-(2',6'-dimethylphenyl)-2-propanone (205826-75-1)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 3,6-di-tert-butyl-9-(2-(dicyclohexylphosphanyl)phenyl)-9H-carbazole; In dichloromethane; at 20 - 90 ℃; for 18.0833h; Schlenk technique;

Reference yield: 84.0%

2,6-dimethyl-1-chlorobenzene (6781-98-2) + acetone (67-64-1) → 1-(2',6'-dimethylphenyl)-2-propanone (205826-75-1)

Guidance literature:

With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; 2-methoxy-6-(N-methyl-N-phenyl-amino)phenyl(dicyclohexyl)phosphine; caesium carbonate; at 90 ℃; for 22.3h; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1002/adsc.201300207

Reference yield:

acetone enolate ion (24262-31-5) + 2,6-dimethyliodobenzene (608-28-6) + diethyl phosphite (29800-93-9) → diethyl 2,6-dimethylphenylphosphonate (54057-96-4) + 1-(2',6'-dimethylphenyl)-2-propanone (205826-75-1)

Guidance literature:

In ammonia; at -33 ℃; Product distribution; Irradiation; competitive reaction, at known concentrations; relative rate constants, half life;

DOI:10.1016/S0040-4020(01)97188-1

upstream raw materials:

acetone enolate ion

2,6-dimethyliodobenzene

diethyl phosphite

2,6-dimethyl-1-chlorobenzene

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