2-[(Piperidin-4-yl)oxy]anisole hydrochloride, 1-Methoxy-2-[(piperidin-4-yl)oxy]benzene hydrochloride

Base Information

• Chemical Name: 2-[(Piperidin-4-yl)oxy]anisole hydrochloride, 1-Methoxy-2-[(piperidin-4-yl)oxy]benzene hydrochloride
• CAS No.: 950649-22-6
• Molecular Formula: C₁₂H₁₇NO₂*ClH
• Molecular Weight: 243.733
• Hs Code.: 2933399990
• Mol file: 950649-22-6.mol

Synonyms:

Chemical Property of 2-[(Piperidin-4-yl)oxy]anisole hydrochloride, 1-Methoxy-2-[(piperidin-4-yl)oxy]benzene hydrochloride

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

4-(2-Methoxyphenoxy)piperidinehydrochloride 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[(Piperidin-4-yl)oxy]anisole hydrochloride, 1-Methoxy-2-[(piperidin-4-yl)oxy]benzene hydrochloride

There total 3 articles about 2-[(Piperidin-4-yl)oxy]anisole hydrochloride, 1-Methoxy-2-[(piperidin-4-yl)oxy]benzene hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 4-(2-methoxyphenoxy)piperidine-1-carboxylate (944808-11-1) → 4-(2-methoxyphenoxy)-piperidine hydrochloride (950649-22-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 25 ℃; for 2h;

DOI:10.1021/jm070219p

Reference yield:

2-methoxy-phenol (90-05-1) → 4-(2-methoxyphenoxy)-piperidine hydrochloride (950649-22-6)

Guidance literature:

Multi-step reaction with 2 steps

1: triphenylphosphine; di-tert-butyl azodicarboxylate / tetrahydrofuran / 0.5 h / 25 °C

2: HCl / dioxane / 2 h / 25 °C

With hydrogenchloride; di-tert-butyl-diazodicarboxylate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; 1: Mitsunobu reaction;

DOI:10.1021/jm070219p

Reference yield:

t-butyl 4-hydroxy piperidine-1-carboxylate (109384-19-2) → 4-(2-methoxyphenoxy)-piperidine hydrochloride (950649-22-6)

Guidance literature:

Multi-step reaction with 2 steps

1: triphenylphosphine; di-tert-butyl azodicarboxylate / tetrahydrofuran / 0.5 h / 25 °C

2: HCl / dioxane / 2 h / 25 °C

With hydrogenchloride; di-tert-butyl-diazodicarboxylate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; 1: Mitsunobu reaction;

DOI:10.1021/jm070219p

upstream raw materials:

tert-butyl 4-(2-methoxyphenoxy)piperidine-1-carboxylate

2-methoxy-phenol

t-butyl 4-hydroxy piperidine-1-carboxylate

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