C₂₄H₂₄O₄

Base Information

Chemical Name:C₂₄H₂₄O₄
CAS No.:1294481-17-6
Molecular Formula:C₂₄H₂₄O₄
Molecular Weight:376.452
Hs Code.:

C<sub>24</sub>H<sub>24</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₄O₄

Chemical Property:

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Technology Process of C₂₄H₂₄O₄

There total 3 articles about C₂₄H₂₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₀O₃

: C₂₄H₂₄O₄

: 1294481-17-6
C₂₄H₂₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; Dess-Martin periodane / dichloromethane / 4 h / 0 °C

2: piperidine; acetic acid / benzene / 2 h / Reflux; Dean-Stark trap

With piperidine; pyridine; Dess-Martin periodane; acetic acid; In dichloromethane; benzene; 2: Knoevenagel condensation;
DOI:10.1021/ja111504w

Reference yield:

: 113388-95-7
3,4,5,6-tetrahydro-[1,1′-biphenyl]-2-carbaldehyde

: C₂₄H₂₄O₄

: 1294481-17-6
C₂₄H₂₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

2.1: pyridine; Dess-Martin periodane / dichloromethane / 4 h / 0 °C

3.1: piperidine; acetic acid / benzene / 2 h / Reflux; Dean-Stark trap

With piperidine; pyridine; n-butyllithium; Dess-Martin periodane; acetic acid; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; benzene; 3.1: Knoevenagel condensation;
DOI:10.1021/ja111504w

Reference yield:

: 1333259-30-5
C₁₆H₁₈O₃

: 123-11-5
4-methoxy-benzaldehyde

: C₂₄H₂₄O₄

: 1294481-17-6
C₂₄H₂₄O₄

Guidance literature:: With piperidine; acetic acid; In benzene; for 2h; optical yield given as %de; Reflux; Dean-Stark trap;
DOI:10.1021/ja111504w