[(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Tb]

Base Information

Chemical Name:[(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Tb]
CAS No.:1269772-10-2
Molecular Formula:C₂₃H₃₈F₃N₅O₇P₃Tb
Molecular Weight:805.426
Hs Code.:

[(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Tb]

Synonyms:

Suppliers and Price of [(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Tb]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Tb]

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Tb]

There total 2 articles about [(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Tb] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1269772-27-1
[(4,7-bis{[hydroxy(methyl)phosphoryl]methyl}-10-({[2-(trifluoromethyl)phenyl]carbamoyl}methyl)-1,4,7,10-tetraazacyclododecan-1-yl)methyl](methyl)phosphinic acid

: 10042-88-3
terbium(III) chloride

: 1269772-10-2
[(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Tb]

Guidance literature:: With NaOH; In water; dissolving C compd. in water, acidification to pH 6, addn. of Tb compd.,heating under reflux for 3 h, cooling, increase of pH to 9.5 with addn. of soln. of NaOH; centrifugation, chromy. (alumina, CH2Cl2/10 % MeOH);
DOI:10.1039/c0dt01232g

Reference yield:

: 1269772-27-1
[(4,7-bis{[hydroxy(methyl)phosphoryl]methyl}-10-({[2-(trifluoromethyl)phenyl]carbamoyl}methyl)-1,4,7,10-tetraazacyclododecan-1-yl)methyl](methyl)phosphinic acid

: terbium(III) acetate

: 1269772-10-2
[(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Tb]

Guidance literature:: With NaOH; In water; dissolving C compd. in water, acidification to pH 6, addn. of Tb compd.,heating under reflux for 3 h, cooling, increase of pH to 9.5 with addn. of soln. of NaOH; centrifugation, chromy. (alumina, CH2Cl2/10 % MeOH);
DOI:10.1039/c0dt01232g