1,4-bis[1'-(pentafluorophenyl)ferrocen-1-yl]tetrafluorobenzene

Base Information

• Chemical Name: 1,4-bis[1'-(pentafluorophenyl)ferrocen-1-yl]tetrafluorobenzene
• CAS No.: 263571-86-4
• Molecular Formula: C₃₈H₁₆F₁₄Fe₂
• Molecular Weight: 850.217
• Mol file: 263571-86-4.mol

Synonyms:

Chemical Property of 1,4-bis[1'-(pentafluorophenyl)ferrocen-1-yl]tetrafluorobenzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1,4-bis[1'-(pentafluorophenyl)ferrocen-1-yl]tetrafluorobenzene

There total 1 articles about 1,4-bis[1'-(pentafluorophenyl)ferrocen-1-yl]tetrafluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

1,1'-dilithioferrocene (33272-09-2) + Hexafluorobenzene (392-56-3) → bis[η(5)-(pentafluorophenyl)cyclopentadienyl]iron(II) (55517-82-3) + 1,4-bis[1'-(pentafluorophenyl)ferrocen-1-yl]tetrafluorobenzene (263571-86-4)

Guidance literature:

In tetrahydrofuran; 1 equiv. of C6F6 was added to ferrocene complex in THF under inert atmosphere at 25 °C, mixt. was stirred for 1 d, water was added; ppt. was filtered, washed with water and dried under vac., extd. with hexane for 12 h, ext. was evapd., solid was washed with hexane 3 times at 25 °C, residue was recrystd. from benzene, elem. anal.;

DOI:10.1021/om990930v

upstream raw materials:

1,1'-dilithioferrocene

Hexafluorobenzene