[6-PPh3-7-Me-μ-(9,10-HMeC)-nido-7-CB10H9]

Base Information

Chemical Name:[6-PPh3-7-Me-μ-(9,10-HMeC)-nido-7-CB10H9]
CAS No.:725734-67-8
Molecular Formula:C₂₂H₃₁B₁₀P
Molecular Weight:434.572
Hs Code.:

Synonyms:

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Chemical Property of [6-PPh3-7-Me-μ-(9,10-HMeC)-nido-7-CB10H9]

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Technology Process of [6-PPh3-7-Me-μ-(9,10-HMeC)-nido-7-CB10H9]

There total 3 articles about [6-PPh3-7-Me-μ-(9,10-HMeC)-nido-7-CB10H9] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 13965-03-2
bis-triphenylphosphine-palladium(II) chloride

: [NHMe3][7-Me-μ-(9,10-HMeC)-nido-7-CB10H10]

: 725734-67-8
[6-PPh3-7-Me-μ-(9,10-HMeC)-nido-7-CB10H9]

: 725734-66-7
[5-PPh3-7-Me-μ-(9,10-HMeC)-nido-7-CB10H9]

Guidance literature:: In ethanol; byproducts: H(1-); (N2); refluxing a soln. of boron compd. and palladium complex in ethanolovernight; filtration through a plug of silica gel, concn., preparative thin layer chromy. (silica gel, CH2Cl2/hexane, 75/25, then 20/80), slow evapn. of layered hexane/CDCl3 soln.;
DOI:10.1021/om030487v

Reference yield: 4.0%

: 13965-03-2
bis-triphenylphosphine-palladium(II) chloride

: 64-17-5
ethanol

: [NHMe3][7-Me-μ-(9,10-HMeC)-nido-7-CB10H10]

: 603-35-0
triphenylphosphine

: [2-Me-3-(CHMe(PPh₃))-closo-2-monocarbaundecaborane]

: 725734-67-8
[6-PPh3-7-Me-μ-(9,10-HMeC)-nido-7-CB10H9]

: 725734-66-7
[5-PPh3-7-Me-μ-(9,10-HMeC)-nido-7-CB10H9]

: [7-Me-8-OEt-9-(CHMe(PPh₃))-nido-7-monocarbaundecaborane]

Guidance literature:: In ethanol; byproducts: H(1-); (N2); refluxing a soln. of boron compd. and palladium complex and phosphine in ethanol for 24 h; filtration, concn., preparative thin layer chromy. (CH2Cl2/hexane 80/20);
DOI:10.1021/om030487v