acetonide of 2-(methylthio)-3-phenylpropane-1,3-diol

Base Information

Chemical Name:acetonide of 2-(methylthio)-3-phenylpropane-1,3-diol
CAS No.:131491-19-5
Molecular Formula:C₁₃H₁₈O₂S
Molecular Weight:238.351
Hs Code.:

Synonyms:

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Chemical Property of acetonide of 2-(methylthio)-3-phenylpropane-1,3-diol

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Technology Process of acetonide of 2-(methylthio)-3-phenylpropane-1,3-diol

There total 4 articles about acetonide of 2-(methylthio)-3-phenylpropane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 131491-19-5,131491-20-8
acetonide of 2-(methylthio)-3-phenylpropane-1,3-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) lithium diisopropylamide / 1) THF, -78 deg C, 2 h, 2) THF, -78 deg C, 1h

2: 1) LiAlH₄, 2) p-TsOH / 1) ether, -78 deg C, 5 h, 2) CH₂Cl₂, 24 h

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; lithium diisopropyl amide;
DOI:10.1021/jo00002a054

Reference yield:

: 100-52-7
benzaldehyde

: 131491-19-5,131491-20-8
acetonide of 2-(methylthio)-3-phenylpropane-1,3-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) lithium diisopropylamide / 1) THF, -78 deg C, 2 h, 2) THF, -78 deg C, 1h

2: 1) LiAlH₄, 2) p-TsOH / 1) ether, -78 deg C, 5 h, 2) CH₂Cl₂, 24 h

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; lithium diisopropyl amide;
DOI:10.1021/jo00002a054

Reference yield:

: 41769-17-9
methyl 2-(methylthio)-3-hydroxy-3-phenylpropionate

: 77-76-9
2,2-dimethoxy-propane

: 131491-19-5,131491-20-8
acetonide of 2-(methylthio)-3-phenylpropane-1,3-diol

: 131491-19-5,131491-20-8
acetonide of 2-(methylthio)-3-phenylpropane-1,3-diol

Guidance literature:: With lithium aluminium tetrahydride; toluene-4-sulfonic acid; Yield given. Multistep reaction. Yields of byproduct given; 1) ether, -78 deg C, 5 h, 2) CH₂Cl₂, 24 h;
DOI:10.1021/jo00002a054