Yb(C₅H₅)2(C₆H₃(CH₃)2NCCH₃CHCCH₃NC₆H₃(CH₃)2)

Base Information

Chemical Name:Yb(C₅H₅)2(C₆H₃(CH₃)2NCCH₃CHCCH₃NC₆H₃(CH₃)2)
CAS No.:604806-65-7
Molecular Formula:C₃₁H₃₅N₂Yb
Molecular Weight:608.672
Hs Code.:

Yb(C<sub>5</sub>H<sub>5</sub>)2(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2NCCH<sub>3</sub>CHCCH<sub>3</sub>NC<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)

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Chemical Property of Yb(C₅H₅)2(C₆H₃(CH₃)2NCCH₃CHCCH₃NC₆H₃(CH₃)2)

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Technology Process of Yb(C₅H₅)2(C₆H₃(CH₃)2NCCH₃CHCCH₃NC₆H₃(CH₃)2)

There total 2 articles about Yb(C₅H₅)2(C₆H₃(CH₃)2NCCH₃CHCCH₃NC₆H₃(CH₃)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 10361-91-8
ytterbium(III) chloride

: 482323-03-5,604806-75-9
lithium N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminate

: sodium cyclopentadienide

: 604806-65-7
Yb(C₅H₅)2(C₆H₃(CH₃)2NCCH₃CHCCH₃NC₆H₃(CH₃)2)

Guidance literature:: In tetrahydrofuran; hexane; toluene; soln. of ligand in toluene-hexane was slowly added to suspn. of YbCl3 inTHF at room temp., THF soln. of NaC5H5 was added, stirred for 48 h at r oom temp. under Ar; centrifuged, THF was removed in vac., ether was added, centrifuged, concd. ether soln. at -10°C;
DOI:10.1016/S0022-328X(03)00453-4

Reference yield: 32.0%

: 604806-61-3
YbCl₂(C₄H₈O)2(C₆H₃(CH₃)2NCCH₃CHCCH₃NC₆H₃(CH₃)2)

: sodium cyclopentadienide

: 604806-65-7
Yb(C₅H₅)2(C₆H₃(CH₃)2NCCH₃CHCCH₃NC₆H₃(CH₃)2)

Guidance literature:: In tetrahydrofuran; NaC5H5 in THF was slowly added to THF susnp. of Yb-complex at room temp., stirred for 24 h under Ar; centrifuged, solvent was evapd. under reduced pressure, ether was added,centrifuged, concd. ether soln. at -10°C for 3 d; elem. anal.;
DOI:10.1016/S0022-328X(03)00453-4