methyl 5-deoxy-5-[(2-hydroxyethyl)amino]-2,3-O-(1-methylethylidene)pentofuranoside

Base Information

Chemical Name:methyl 5-deoxy-5-[(2-hydroxyethyl)amino]-2,3-O-(1-methylethylidene)pentofuranoside
CAS No.:6329-22-2
Molecular Formula:C₁₁H₂₁NO₅
Molecular Weight:247.291
Hs Code.:

Synonyms:Ribofuranoside,methyl 5-deoxy-5-[(2-hydroxyethyl)amino]-2,3-O-isopropylidene- (7CI);Furo[3,4-d]-1,3-dioxole, b-D-ribofuranoside deriv.; NSC 43416

Suppliers and Price of methyl 5-deoxy-5-[(2-hydroxyethyl)amino]-2,3-O-(1-methylethylidene)pentofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of methyl 5-deoxy-5-[(2-hydroxyethyl)amino]-2,3-O-(1-methylethylidene)pentofuranoside

Chemical Property:

Vapor Pressure:5.37E-07mmHg at 25°C
Boiling Point:370.4°C at 760 mmHg
Flash Point:177.8°C
Density:1.2g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 5-deoxy-5-[(2-hydroxyethyl)amino]-2,3-O-(1-methylethylidene)pentofuranoside

There total 4 articles about methyl 5-deoxy-5-[(2-hydroxyethyl)amino]-2,3-O-(1-methylethylidene)pentofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 4137-56-8
methyl 2,3-O-isopropylidene-5-O-p-tolylsulfonyl-β-D-ribofuranoside

: 141-43-5
ethanolamine

: 6329-22-2
methyl 5-deoxy-5-(2-hydroxyethylamino)-2,3-O-isopropylidene-β-D-ribofuranoside

Guidance literature:: In ethanol; for 24h; Reflux;
DOI:10.1007/s10534-015-9870-8

Reference yield:

: 7473-45-2
1-O-methyl-D-ribofuranose

: 6329-22-2
methyl 5-deoxy-5-(2-hydroxyethylamino)-2,3-O-isopropylidene-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / methanol; water

2: pyridine

3: ethanol / 24 h / Reflux

With pyridine; hydrogenchloride; In methanol; ethanol; water;
DOI:10.1007/s10534-015-9870-8

Reference yield:

: 4099-85-8,828937-29-7
((3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol

: 6329-22-2
methyl 5-deoxy-5-(2-hydroxyethylamino)-2,3-O-isopropylidene-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: ethanol / 24 h / Reflux

With pyridine; In ethanol;
DOI:10.1007/s10534-015-9870-8