[(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Dy]

Base Information

Chemical Name:[(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Dy]
CAS No.:1269772-14-6
Molecular Formula:C₂₃H₃₈DyF₃N₅O₇P₃
Molecular Weight:809.001
Hs Code.:

[(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Dy]

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Chemical Property of [(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Dy]

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Technology Process of [(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Dy]

There total 1 articles about [(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Dy] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10025-74-8
dysprosium(III) trichloride

: 1269772-27-1
[(4,7-bis{[hydroxy(methyl)phosphoryl]methyl}-10-({[2-(trifluoromethyl)phenyl]carbamoyl}methyl)-1,4,7,10-tetraazacyclododecan-1-yl)methyl](methyl)phosphinic acid

: 1269772-14-6
[(([(4,7-di([hydroxy(methyl)phosphoryl]methyl)-10-(([2-(trifluoromethyl)phenyl]carbamoyl)methyl)-1,4,7,10-tetraazacyclododec-1-yl)methyl](methyl)phosphinic acid)(-3H))Dy]

Guidance literature:: With NaOH; In water; dissolving C compd. in water, acidification to pH 6, addn. of Dy compd.,heating under reflux for 3 h, cooling, increase of pH to 9.5 with addn. of soln. of NaOH; centrifugation, chromy. (alumina, CH2Cl2/10 % MeOH);
DOI:10.1039/c0dt01232g