N-phenyl-P,P,P-trisphospha-λ⁵-azene

Base Information

Chemical Name:N-phenyl-P,P,P-trisphospha-λ⁵-azene
CAS No.:13406-18-3
Molecular Formula:C₂₇H₁₇F₉NP
Molecular Weight:557.398
Hs Code.:

N-phenyl-P,P,P-tris<p-(trifluoromethyl)phenyl>phospha-λ<sup>5</sup>-azene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-P,P,P-trisphospha-λ⁵-azene

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Technology Process of N-phenyl-P,P,P-trisphospha-λ⁵-azene

There total 4 articles about N-phenyl-P,P,P-trisphospha-λ⁵-azene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 402-43-7
p-trifluoromethylphenyl bromide

: 13406-18-3
N-phenyl-P,P,P-trisphospha-λ⁵-azene

Guidance literature:: Multi-step reaction with 2 steps

1: 2) PCl₃ / 2) Et₂O, reflux, 1h

2: 1) Br₂, 2) Et₃N / 1) benzene, 6 to 8 deg C, 20 min, 2) r.t., 4h

With bromine; triethylamine; phosphorus trichloride;
DOI:10.1021/jo00008a036

Reference yield:

: 62-53-3
aniline

: 13406-29-6
tris(para-trifluoromethyl)phenyl phosphine

: 13406-18-3
N-phenyl-P,P,P-trisphospha-λ⁵-azene

Guidance literature:: With bromine; triethylamine; Yield given. Multistep reaction; 1) benzene, 6 to 8 deg C, 20 min, 2) r.t., 4h;
DOI:10.1021/jo00008a036