(diisopropylamino)methyl(2-methylbenzyl)borane

Base Information

Chemical Name:(diisopropylamino)methyl(2-methylbenzyl)borane
CAS No.:150480-14-1
Molecular Formula:C₁₅H₂₆BN
Molecular Weight:231.189
Hs Code.:

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Chemical Property of (diisopropylamino)methyl(2-methylbenzyl)borane

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Technology Process of (diisopropylamino)methyl(2-methylbenzyl)borane

There total 2 articles about (diisopropylamino)methyl(2-methylbenzyl)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 75-77-4
chloro-trimethyl-silane

: 150480-06-1
diisopropylamino-2-boraindane

: 150480-14-1
(diisopropylamino)methyl(2-methylbenzyl)borane

: 2-(diisopropylamino)-1,3-bis(trimethylsilyl)-2-boraindane

Guidance literature:: In pentane; 22.4 mmol LiCH3 (in ether, 1.6 M) was added dropwise to a soln. of 24 mmol C6H4(CH2)2BN(CH(CH3)2)2 in pentane at -78°C; the mixed was allowed to warm up to 20°C and stirred for 12 h;; removal of volatiles in vac.; condensation (1E-5 bar/100°C) of the less volatile fraction yields prod. contaminated with educt; addn. of (CH3)3SiCl to residue and distn. (high vac.) yields C6H4(CHSiMe3)2BN(CH(CH3)2)2 isomer ratio 2:1 (trans/cis);;

Reference yield:

: 44873-49-6
(diisopropylamino)dichloroborane

: 150480-14-1
(diisopropylamino)methyl(2-methylbenzyl)borane

: 2-(diisopropylamino)-1,3-bis(trimethylsilyl)-2-boraindane

Guidance literature:: Multi-step reaction with 2 steps

1: KOC(CH₃)3; LiC₄H₉ / hexane

2: pentane

With KOC(CH₃)3; LiC₄H₉; In hexane; pentane;