Technology Process of C16H20ClNO6S
There total 3 articles about C16H20ClNO6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: formic acid / water / 6 h / 75 °C
2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
3: dihydrogen peroxide; palladium diacetate; acetic acid; calcium chloride / water / 20 °C
With
formic acid; dihydrogen peroxide; palladium diacetate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; calcium chloride;
In
tetrahydrofuran; water;
DOI:10.1002/chem.201102776
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
2: dihydrogen peroxide; palladium diacetate; acetic acid; calcium chloride / water / 20 °C
With
dihydrogen peroxide; palladium diacetate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; calcium chloride;
In
tetrahydrofuran; water;
DOI:10.1002/chem.201102776
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
2: dihydrogen peroxide; palladium diacetate; acetic acid; calcium chloride / water / 20 °C
With
dihydrogen peroxide; palladium diacetate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; calcium chloride;
In
tetrahydrofuran; water;
DOI:10.1002/chem.201102776
