Technology Process of C13H18N2
There total 4 articles about C13H18N2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanol / 0.75 h / 20 °C
2: nickel/aluminium alloy; sodium hydroxide / ethanol; water / 5 h
3: edetate disodium; mercury(II) oxide / water / 1 h / Reflux; Inert atmosphere
With
nickel/aluminium alloy; edetate disodium; mercury(II) oxide; sodium hydroxide;
In
methanol; ethanol; water;
DOI:10.1691/ph.2009.9564
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydroxylamine hydrochloride
2: methanol / 0.75 h / 20 °C
3: nickel/aluminium alloy; sodium hydroxide / ethanol; water / 5 h
4: edetate disodium; mercury(II) oxide / water / 1 h / Reflux; Inert atmosphere
With
nickel/aluminium alloy; hydroxylamine hydrochloride; edetate disodium; mercury(II) oxide; sodium hydroxide;
In
methanol; ethanol; water;
DOI:10.1691/ph.2009.9564
- Guidance literature:
-
Multi-step reaction with 2 steps
1: nickel-aluminum alloy; sodium hydroxide / ethanol; water / 5 h
2: edetate disodium; mercury(II) oxide / water / 1 h / Reflux; Inert atmosphere
With
nickel-aluminum alloy; edetate disodium; mercury(II) oxide; sodium hydroxide;
In
ethanol; water;
DOI:10.1691/ph.2009.9564