hexakis(ethyl isocyanoacetato)technetium(I) tetraphenylboranate

Base Information

Chemical Name:hexakis(ethyl isocyanoacetato)technetium(I) tetraphenylboranate
CAS No.:121310-03-0
Molecular Formula:C₂₄H₂₀B*C₃₀H₄₂N₆O₁₂Tc
Molecular Weight:1095.84
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexakis(ethyl isocyanoacetato)technetium(I) tetraphenylboranate

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Technology Process of hexakis(ethyl isocyanoacetato)technetium(I) tetraphenylboranate

There total 2 articles about hexakis(ethyl isocyanoacetato)technetium(I) tetraphenylboranate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: hexakis(thioureato)technetium(III) chloride

: 2999-46-4
Ethyl isocyanoacetate

: 143-66-8
sodium tetraphenyl borate

: 121310-03-0
hexakis(ethyl isocyanoacetato)technetium(I) tetraphenylboranate

Guidance literature:: In methanol; water; Tc complex dissolved in MeOH was treated with isocyanoacetate and refluxed for 3 h; solvent vol. reduced to ca. 10 ml and dild. with water, thenpptd. with satd. aq. NaBPh4 soln.; ppt. centrifuged, recrystd. from acetone/water; elem. anal.;

Reference yield:

: 2999-46-4
Ethyl isocyanoacetate

: 23288-61-1
pertechnetate anion

: 121310-03-0
hexakis(ethyl isocyanoacetato)technetium(I) tetraphenylboranate

Guidance literature:: With Na₂S₂O₄; NaOH; In sodium hydroxide; aq. NaOH; redn. of pertechnate with dithionite in presence of isocyanoacetate in 0.05 N NaOH;