YbCl([N(SiMe3)C(Ph)]2CH)(μ-Cl)2Li(OEt2)2*Et2O

Base Information

Chemical Name:YbCl([N(SiMe3)C(Ph)]2CH)(μ-Cl)2Li(OEt2)2*Et2O
CAS No.:1196390-10-9
Molecular Formula:C₄H₁₀O*C₄₁H₅₇Cl₃LiN₂O₂Si₂Yb
Molecular Weight:1026.55
Hs Code.:

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Chemical Property of YbCl([N(SiMe3)C(Ph)]2CH)(μ-Cl)2Li(OEt2)2*Et2O

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Technology Process of YbCl([N(SiMe3)C(Ph)]2CH)(μ-Cl)2Li(OEt2)2*Et2O

There total 1 articles about YbCl([N(SiMe3)C(Ph)]2CH)(μ-Cl)2Li(OEt2)2*Et2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 10361-91-8
ytterbium(III) chloride

: 60-29-7,927820-24-4
diethyl ether

: Li([N(SiMe₃)C(C₆H₄Ph-4)]2CH)*thf

: 1196390-10-9
YbCl([N(SiMe3)C(Ph)]2CH)(μ-Cl)2Li(OEt2)2*Et2O

Guidance literature:: In tetrahydrofuran; under Ar or in vac.; YbCl3 added to stirred soln. of Li(β-diiminatoligand) in THF, yellow soln. kept at room temp. for 24 h, volatiles rem oved in vac., solid residue extd. with Et2O; ext. concd., cooled to -27°C, yellow crystals obtained; XRD;
DOI:10.1016/j.ica.2009.06.025