1-(β-(ferrocenylthio)ethyl)-3-(2,4,6-trimethylphenyl)imidazolium iodide

Base Information

Chemical Name:1-(β-(ferrocenylthio)ethyl)-3-(2,4,6-trimethylphenyl)imidazolium iodide
CAS No.:1338782-00-5
Molecular Formula:C₂₄H₂₇FeN₂S*I
Molecular Weight:558.309
Hs Code.:

Synonyms:

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Chemical Property of 1-(β-(ferrocenylthio)ethyl)-3-(2,4,6-trimethylphenyl)imidazolium iodide

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Technology Process of 1-(β-(ferrocenylthio)ethyl)-3-(2,4,6-trimethylphenyl)imidazolium iodide

There total 1 articles about 1-(β-(ferrocenylthio)ethyl)-3-(2,4,6-trimethylphenyl)imidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 227175-39-5
(2-chloroethylthio)ferrocene

: 25364-44-7
N-(2,4,6-trimethylphenyl)imidazole

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 1338782-00-5
1-(β-(ferrocenylthio)ethyl)-3-(2,4,6-trimethylphenyl)imidazolium iodide

Guidance literature:: In acetonitrile; (inert atm.); heating mixt. of ferrocene deriv., NaI and imidazole deriv. in degassed CH3CN at 80°C for 16 h; cooling to room temp., evapn. (CH2Cl2), filtration through celite, concg., addn. of diethyl ether, filtration through celite, washing with ether, extn. (CH2Cl2), evapn., NMR;
DOI:10.1039/c1nj20224c

Reference yield:

: 13755-29-8
sodium tetrafluoroborate

: 1338782-00-5
1-(β-(ferrocenylthio)ethyl)-3-(2,4,6-trimethylphenyl)imidazolium iodide

: 1338782-07-2
1-(β-(ferrocenylthio)ethyl)-3-(2,4,6-trimethylphenyl)imidazolium tetrafluoroborate

Guidance literature:: In dichloromethane; water; (inert atm.); addn. of aq. soln. of NaBF4 to CH2Cl2 soln. of ferrocene deriv., stirring for 16 h; separation organic phase, extn. (CH2Cl2), washing combined CH2Cl2 solns.with water, drying over Na2SO4, filtration, concg., addn. of ether, fil tration through celite, washing with ether, extn. (CH2Cl2), evapn., elem. anal.;
DOI:10.1039/c1nj20224c