Technology Process of C48H62N8O11S
There total 4 articles about C48H62N8O11S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium azide / ethanol / 20 - 70 °C
2: triethylamine / dichloromethane / 6 h / 20 - 22 °C
3: potassium carbonate / N,N-dimethyl-formamide / 20 - 80 °C
4: hydroxylamine hydrochloride; triethylamine / dichloromethane / 20 - 22 °C
5: methanol / 3 h / 20 - 22 °C
With
sodium azide; hydroxylamine hydrochloride; potassium carbonate; triethylamine;
In
methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja1081519
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / tetrahydrofuran / 2 h / 0 °C
2: sodium azide / ethanol / 20 - 70 °C
3: triethylamine / dichloromethane / 6 h / 20 - 22 °C
4: potassium carbonate / N,N-dimethyl-formamide / 20 - 80 °C
5: hydroxylamine hydrochloride; triethylamine / dichloromethane / 20 - 22 °C
6: methanol / 3 h / 20 - 22 °C
With
sodium azide; hydroxylamine hydrochloride; potassium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja1081519
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 6 h / 20 - 22 °C
2: potassium carbonate / N,N-dimethyl-formamide / 20 - 80 °C
3: hydroxylamine hydrochloride; triethylamine / dichloromethane / 20 - 22 °C
4: methanol / 3 h / 20 - 22 °C
With
hydroxylamine hydrochloride; potassium carbonate; triethylamine;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja1081519