7c-methyl-7t-[N'-(1-methyl-1-phenyl-ethoxycarbonyl)-hydrazinocarbonyl]-8-oxo-(6rH)-4-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid tert-butyl ester

Base Information

Chemical Name:7c-methyl-7t-[N'-(1-methyl-1-phenyl-ethoxycarbonyl)-hydrazinocarbonyl]-8-oxo-(6rH)-4-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid tert-butyl ester
CAS No.:37469-77-5
Molecular Formula:C₂₃H₃₁N₃O₆S
Molecular Weight:477.582
Hs Code.:

7<i>c</i>-methyl-7<i>t</i>-[<i>N</i>'-(1-methyl-1-phenyl-ethoxycarbonyl)-hydrazinocarbonyl]-8-oxo-(6<i>r</i><i>H</i>)-4-thia-1-aza-bicyclo[4.2.0]octane-2<i>c</i>-carboxylic acid <i>tert</i>-butyl ester

Synonyms:

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Chemical Property of 7c-methyl-7t-[N'-(1-methyl-1-phenyl-ethoxycarbonyl)-hydrazinocarbonyl]-8-oxo-(6rH)-4-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid tert-butyl ester

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Technology Process of 7c-methyl-7t-[N'-(1-methyl-1-phenyl-ethoxycarbonyl)-hydrazinocarbonyl]-8-oxo-(6rH)-4-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid tert-butyl ester

There total 1 articles about 7c-methyl-7t-[N'-(1-methyl-1-phenyl-ethoxycarbonyl)-hydrazinocarbonyl]-8-oxo-(6rH)-4-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18597-93-8
cumyl carbazate

: 49855-64-3
7-methyl-8-oxo-(6rH)-4-thia-1-aza-bicyclo[4.2.0]octane-2c,7t-dicarboxylic acid 2-tert-butyl ester

: 37469-77-5,49855-65-4
7c-methyl-7t-[N'-(1-methyl-1-phenyl-ethoxycarbonyl)-hydrazinocarbonyl]-8-oxo-(6rH)-4-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid tert-butyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/P19730001321

Reference yield:

: 37469-77-5,49855-65-4
7c-methyl-7t-[N'-(1-methyl-1-phenyl-ethoxycarbonyl)-hydrazinocarbonyl]-8-oxo-(6rH)-4-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid tert-butyl ester

: 37469-83-3,49855-71-2
7c-methyl-8-oxo-7t-(2-phenyl-acetylamino)-(6rH)-4-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: (i) HCl_. CH₂Cl₂, (ii) aq. HCl, NaNO₂, (iii) benzene, (iv) /BRN= 906698/

2: (i) CF₃CO₂H, (ii) NaHCO₃, /BRN= 742254/, acetone

3: (i) Et₃N, aq. CH₂Cl₂, (ii) /BRN= 970619/, (iii) Py

4: (i) Cl₂, CCl₄, (ii) Py

5: Zn, aq. AcOH

With acetic acid; zinc;
DOI:10.1039/P19730001321

Reference yield:

: 37469-77-5,49855-65-4
7c-methyl-7t-[N'-(1-methyl-1-phenyl-ethoxycarbonyl)-hydrazinocarbonyl]-8-oxo-(6rH)-4-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid tert-butyl ester

: 37469-80-0,49855-68-7
7c-methyl-8-oxo-7t-(2-phenyl-acetylamino)-(6rH)-4-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: (i) HCl_. CH₂Cl₂, (ii) aq. HCl, NaNO₂, (iii) benzene, (iv) /BRN= 906698/

2: (i) CF₃CO₂H, (ii) NaHCO₃, /BRN= 742254/, acetone

DOI:10.1039/P19730001321