Technology Process of C33H39N5O2
There total 10 articles about C33H39N5O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h / 20 °C
2: Microwave irradiation
With
N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran;
DOI:10.1039/c7md00052a
- Guidance literature:
-
Multi-step reaction with 8 steps
1: potassium carbonate / 20 °C
2: acetic anhydride; nitric acid / 18 h / 20 °C
3: iron; ammonium chloride / water; isopropyl alcohol / 18 h / Reflux
4: acetic acid / water / 18 h / 20 °C
5: sodium hydroxide / methanol; water / 6 h / pH 13 / Reflux
6: trichlorophosphate; N-ethyl-N,N-diisopropylamine / acetonitrile / 6 h / Reflux
7: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h / 20 °C
8: Microwave irradiation
With
nitric acid; acetic anhydride; iron; potassium carbonate; ammonium chloride; acetic acid; N-ethyl-N,N-diisopropylamine; sodium hydroxide; trichlorophosphate;
In
tetrahydrofuran; methanol; water; isopropyl alcohol; acetonitrile;
DOI:10.1039/c7md00052a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / methanol; water / 6 h / pH 13 / Reflux
2: trichlorophosphate; N-ethyl-N,N-diisopropylamine / acetonitrile / 6 h / Reflux
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h / 20 °C
4: Microwave irradiation
With
N-ethyl-N,N-diisopropylamine; sodium hydroxide; trichlorophosphate;
In
tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1039/c7md00052a
