N'-(4-(tert-butyldimethylsilyloxy)benzyl)-fluorenylmethyl carbazate

Base Information

• Chemical Name: N'-(4-(tert-butyldimethylsilyloxy)benzyl)-fluorenylmethyl carbazate
• CAS No.: 869291-41-8
• Molecular Formula: C₂₈H₃₄N₂O₃Si
• Molecular Weight: 474.675
• Mol file: 869291-41-8.mol

Synonyms:

Chemical Property of N'-(4-(tert-butyldimethylsilyloxy)benzyl)-fluorenylmethyl carbazate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N'-(4-(tert-butyldimethylsilyloxy)benzyl)-fluorenylmethyl carbazate

There total 1 articles about N'-(4-(tert-butyldimethylsilyloxy)benzyl)-fluorenylmethyl carbazate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(9-fluorenylmethyloxycarbonyl)hydrazine (35661-51-9) + p-[(tert-butyldimethylsilyl)oxy]benzaldehyde (120743-99-9) → N'-(4-(tert-butyldimethylsilyloxy)benzyl)-fluorenylmethyl carbazate (869291-41-8)

Guidance literature:

N-(9-fluorenylmethyloxycarbonyl)hydrazine; p-[(tert-butyldimethylsilyl)oxy]benzaldehyde; In ethanol; Reflux;

With hydrogen; palladium(II) hydroxide; In ethanol;

DOI:10.1021/jm300557t

Reference yield:

phosgene (75-44-5) + N'-(4-(tert-butyldimethylsilyloxy)benzyl)-fluorenylmethyl carbazate (869291-41-8) → C29H33ClN2O4Si

Guidance literature:

In dichloromethane; toluene; at 0 ℃; for 0.25h;

DOI:10.1021/jm300557t

upstream raw materials:

N-(9-fluorenylmethyloxycarbonyl)hydrazine

p-[(tert-butyldimethylsilyl)oxy]benzaldehyde