tris(p-nonafluorobiphenyl)boron acetonitrile

Base Information

Chemical Name:tris(p-nonafluorobiphenyl)boron acetonitrile
CAS No.:1144521-94-7
Molecular Formula:C₃₈H₃BF₂₇N
Molecular Weight:997.216
Hs Code.:

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Chemical Property of tris(p-nonafluorobiphenyl)boron acetonitrile

Chemical Property:

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Technology Process of tris(p-nonafluorobiphenyl)boron acetonitrile

There total 2 articles about tris(p-nonafluorobiphenyl)boron acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 252684-48-3
tris(p-nonafluorobiphenyl)boron

: 75-05-8,26809-02-9
acetonitrile

: 1144521-94-7
tris(p-nonafluorobiphenyl)boron acetonitrile

Guidance literature:: In light petroleum; at -27 ℃; Inert atmosphere;
DOI:10.1039/b817252h

Reference yield:

: 1038-65-9
4-bromo-2,2',3,3',4',5,5',6,6'-nonafluoro-1,1'-biphenyl

: 10294-34-5
boron trichloride

: 75-05-8,26809-02-9
acetonitrile

: 1144521-94-7
tris(p-nonafluorobiphenyl)boron acetonitrile

Guidance literature:: With H₃CCH₂CH₂CH₂Li; In diethyl ether; n-heptane; byproducts: LiCl; (N2), Schlenk technique; dissolving of (C6F5)C6F4Br in diethyl ether andlight petroleum (1:1), cooling to -78°C, dropwise addn. of soln. of C4H9Li in hexane, stirring for 2 h, addn. of soln. of BCl3 in heptan e, slow warming to room temp.; filtration, acetonitrile addn. to the filtrate, evapn. under vacuum, elem. anal.;
DOI:10.1039/b817252h