C₁₅H₁₂⁽²⁾HNS

Base Information

• Chemical Name: C₁₅H₁₂⁽²⁾HNS
• CAS No.: 1351438-41-9
• Molecular Formula: C₁₅H₁₃NS
• Molecular Weight: 240.333
• Mol file: 1351438-41-9.mol

Synonyms:

Chemical Property of C₁₅H₁₂⁽²⁾HNS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₂⁽²⁾HNS

There total 4 articles about C₁₅H₁₂⁽²⁾HNS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethylbenzoyl chloride (6613-44-1) → 2-(3,5-dimethylphenyl)benzo[d]thiazole (152355-90-3) + C15H12(2)HNS (1351438-41-9)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 3 h / 20 °C

2: Lawessons reagent / toluene / 2 h / Reflux; Inert atmosphere

3: graphitic carbon nitride / dimethyl sulfoxide / 10 h / 20 °C / Irradiation

With Lawessons reagent; graphitic carbon nitride; triethylamine; In dichloromethane; dimethyl sulfoxide; toluene;

DOI:10.1021/acs.orglett.1c01571

Reference yield:

2-deuterioaniline (50535-17-6) → 2-(3,5-dimethylphenyl)benzo[d]thiazole (152355-90-3) + C15H12(2)HNS (1351438-41-9)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 3 h / 20 °C

2: Lawessons reagent / toluene / 2 h / Reflux; Inert atmosphere

3: graphitic carbon nitride / dimethyl sulfoxide / 10 h / 20 °C / Irradiation

With Lawessons reagent; graphitic carbon nitride; triethylamine; In dichloromethane; dimethyl sulfoxide; toluene;

DOI:10.1021/acs.orglett.1c01571

Reference yield:

N-(2-deuterium phenyl)-3,5-dimethylbenzothiozamide (1351438-40-8) → 2-(3,5-dimethylphenyl)benzo[d]thiazole (152355-90-3) + C15H12(2)HNS (1351438-41-9)

Guidance literature:

With graphitic carbon nitride; In dimethyl sulfoxide; at 20 ℃; for 10h; Kinetics; Irradiation;

DOI:10.1021/acs.orglett.1c01571

upstream raw materials:

3,5-dimethylbenzoyl chloride

2-bromoaniline

N-(2-deuterium phenyl)-3,5-dimethylbenzothiozamide

2-deuterioaniline