1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-isopropylbenzimidazole

Base Information

• Chemical Name: 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-isopropylbenzimidazole
• CAS No.: 130423-44-8
• Molecular Formula: C₂₄H₃₂N₂O
• Molecular Weight: 364.531
• Mol file: 130423-44-8.mol

Synonyms:

Chemical Property of 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-isopropylbenzimidazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-isopropylbenzimidazole

There total 3 articles about 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-isopropylbenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-Di-tert-butyl-1,4-benzoquinone (719-22-2) → 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-isopropylbenzimidazole (130423-44-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / propan-1-ol / 4 h / Heating

2: 1) reflux, 10 min, 2) 110 deg C, 5 min

In propan-1-ol;

DOI:10.1007/BF00497212

Reference yield:

1,2-diamino-benzene (95-54-5) → 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-isopropylbenzimidazole (130423-44-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / propan-1-ol / 4 h / Heating

2: 1) reflux, 10 min, 2) 110 deg C, 5 min

In propan-1-ol;

DOI:10.1007/BF00497212

Reference yield:

4-((2-aminophenyl)imino)-2,6-di-tert-butylcyclohexa-2,5-dienone (118194-38-0) + isobutyraldehyde (78-84-2) → 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-isopropylbenzimidazole (130423-44-8)

Guidance literature:

1) reflux, 10 min, 2) 110 deg C, 5 min;

DOI:10.1007/BF00497212

upstream raw materials:

4-((2-aminophenyl)imino)-2,6-di-tert-butylcyclohexa-2,5-dienone

isobutyraldehyde

2,6-Di-tert-butyl-1,4-benzoquinone

1,2-diamino-benzene