(RS)-phosphonic acid

Base Information

• Chemical Name: (RS)-phosphonic acid
• CAS No.: 114987-76-7
• Molecular Formula: C₁₁H₁₈NO₃P
• Molecular Weight: 243.243

Synonyms:

Chemical Property of (RS)-phosphonic acid

Chemical Property:

Purity/Quality:

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Technology Process of (RS)-phosphonic acid

There total 2 articles about (RS)-phosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-tert-Butylbenzaldehyde (939-97-9) → (RS)-phosphonic acid (114987-76-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 70.6 percent / Al₂O₃ / 90 °C

With aluminum oxide;

DOI:10.1002/hlca.19870700603

Reference yield:

→ (RS)-phosphonic acid (114987-76-7)

Guidance literature:

entspr. Hydrochlorid, Kochen in Wasser;

DOI:10.1021/jo01272a016

Reference yield:

chloro-trimethyl-silane (75-77-4) + (RS)-phosphonic acid (114987-76-7) + naphthalene-1-carbonic acid chloride (879-18-5) → (RS)-dimethyl <(naphthalene-1-carboxamido)(4-(tert-butyl)phenyl)methyl>phosphonate

Guidance literature:

With pyridine; Yield given. Multistep reaction; 1.) CH₂Cl₂, room temp, 60 min; 2.) MeOH, -25 deg C, 2.5 h;

DOI:10.1002/hlca.19870700603

upstream raw materials:

4-tert-Butylbenzaldehyde

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