S-isopropyl O,O-dimethyl phosphorodithioate

Base Information

• Chemical Name: S-isopropyl O,O-dimethyl phosphorodithioate
• CAS No.: 77547-89-8
• Molecular Formula: C₅H₁₃O₂PS₂
• Molecular Weight: 200.263

Synonyms:

Chemical Property of S-isopropyl O,O-dimethyl phosphorodithioate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of S-isopropyl O,O-dimethyl phosphorodithioate

There total 3 articles about S-isopropyl O,O-dimethyl phosphorodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

O,O-dimethyl dithiophosphoric acid S-trimethylsilyl ester (18135-34-7) + diisopropyl (2-oxopropyl)phosphonate (67257-36-7) + cyclohexylamine (108-91-8,157973-60-9) → cyclohexylammonium isopropyl acetonylphosphonate (77547-88-7) + S-isopropyl O,O-dimethyl phosphorodithioate (77547-89-8)

Guidance literature:

Yield given. Multistep reaction; 1) alcohol, room temp., 2 h; 2) benzene.;

Reference yield:

O,O-dimethyl dithiophosphoric acid S-trimethylsilyl ester (18135-34-7) + cyclohexylamine (108-91-8,157973-60-9) + Dimethyl phosphite (868-85-9) → cyclohexylammonium isopropyl hydrogen phosphite (77547-92-3) + S-isopropyl O,O-dimethyl phosphorodithioate (77547-89-8)

Guidance literature:

Yield given. Multistep reaction; 1) 20-30 deg C; 2) benzen;

Reference yield:

O,O-dimethyl dithiophosphoric acid S-trimethylsilyl ester (18135-34-7) + cyclohexylamine (108-91-8,157973-60-9) + dimethyl methane phosphonate (756-79-6) → cyclohexylammonium isopropyl methylphosphonate (77547-91-2) + S-isopropyl O,O-dimethyl phosphorodithioate (77547-89-8)

Guidance literature:

Yield given. Multistep reaction; 1) 20-30 deg C; 2) benzen;

upstream raw materials:

O,O-dimethyl dithiophosphoric acid S-trimethylsilyl ester

diisopropyl (2-oxopropyl)phosphonate

cyclohexylamine

Dimethyl phosphite

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