methyltriphenylphosphonium fluorobis(4-methylbenzene-1,2-dithiolato)germanate

Base Information

Chemical Name:methyltriphenylphosphonium fluorobis(4-methylbenzene-1,2-dithiolato)germanate
CAS No.:79084-39-2
Molecular Formula:C₁₄H₁₂FGeS₄*C₁₉H₁₈P
Molecular Weight:677.427
Hs Code.:

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Chemical Property of methyltriphenylphosphonium fluorobis(4-methylbenzene-1,2-dithiolato)germanate

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Technology Process of methyltriphenylphosphonium fluorobis(4-methylbenzene-1,2-dithiolato)germanate

There total 1 articles about methyltriphenylphosphonium fluorobis(4-methylbenzene-1,2-dithiolato)germanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: potassium fluoride dihydrate

: 79084-23-4
bis(toluene-3,4-dithiolato)germanium(IV)

: 1779-49-3
Methyltriphenylphosphonium bromide

: 79084-39-2
methyltriphenylphosphonium fluorobis(4-methylbenzene-1,2-dithiolato)germanate

Guidance literature:: In acetonitrile; byproducts: potassium bromide, water; under N2, Ge-complex and KF*2H2O suspd. in soln. of Ph3PMeBr (molar ratio 1:2:1) in MeCN, heated under reflux for 3 h; cooled to room temp., filtered, filtrate concd., cooled to 0°C, recrystd. from MeCN at 0°C; elem. anal.;
DOI:10.1021/ic50226a019