N-(β-Methoxycarbonyl-styryl)-O.O-diphenyl-thiophosphorsaeureamid

Base Information

• Chemical Name: N-(β-Methoxycarbonyl-styryl)-O.O-diphenyl-thiophosphorsaeureamid
• CAS No.: 37390-48-0
• Molecular Formula: C₂₂H₂₀NO₄PS
• Molecular Weight: 425.445
• Mol file: 37390-48-0.mol

Synonyms:

Chemical Property of N-(β-Methoxycarbonyl-styryl)-O.O-diphenyl-thiophosphorsaeureamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(β-Methoxycarbonyl-styryl)-O.O-diphenyl-thiophosphorsaeureamid

There total 2 articles about N-(β-Methoxycarbonyl-styryl)-O.O-diphenyl-thiophosphorsaeureamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-formyl-2-phenylacetate (5894-79-1) + Amidothiophosphorsaeurediphenylester (19326-23-9) → N-(β-Methoxycarbonyl-styryl)-O.O-diphenyl-thiophosphorsaeureamid (37390-48-0)

Guidance literature:

With phosphorus pentoxide; toluene-4-sulfonic acid;

DOI:10.1002/ardp.19723050702

Reference yield:

O,O-diphenyl phosphorochloridothioate (22077-44-7) → N-(β-Methoxycarbonyl-styryl)-O.O-diphenyl-thiophosphorsaeureamid (37390-48-0)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NH₃

2: TsOH, P₂O₅

With ammonium hydroxide; phosphorus pentoxide; toluene-4-sulfonic acid;

DOI:10.1002/ardp.19723050702

upstream raw materials:

methyl 2-formyl-2-phenylacetate

Amidothiophosphorsaeurediphenylester

O,O-diphenyl phosphorochloridothioate

Refernces