1,3,4-Tris-phenylsulfanyl-benzo[4,5]thieno[3,2-c]pyridine; compound with chloro-benzene

Base Information

• Chemical Name: 1,3,4-Tris-phenylsulfanyl-benzo[4,5]thieno[3,2-c]pyridine; compound with chloro-benzene
• CAS No.: 94532-27-1
• Molecular Formula: C₆H₅Cl*2C₂₉H₁₉NS₄
• Molecular Weight: 1132.04
• Mol file: 94532-27-1.mol

Synonyms:

Chemical Property of 1,3,4-Tris-phenylsulfanyl-benzo[4,5]thieno[3,2-c]pyridine; compound with chloro-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,4-Tris-phenylsulfanyl-benzo[4,5]thieno[3,2-c]pyridine; compound with chloro-benzene

There total 3 articles about 1,3,4-Tris-phenylsulfanyl-benzo[4,5]thieno[3,2-c]pyridine; compound with chloro-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,4,5,6-pentachloropyridine (2176-62-7) → 1,3,4-Tris-phenylsulfanyl-benzo[4,5]thieno[3,2-c]pyridine; compound with chloro-benzene (94532-27-1)

Guidance literature:

Multi-step reaction with 2 steps

1: various solvent(s) / Ambient temperature; in normal daylight

In various solvent(s);

DOI:10.1016/S0040-4039(01)81423-4

Reference yield:

sodium thiophenolate (930-69-8) → 1,3,4-Tris-phenylsulfanyl-benzo[4,5]thieno[3,2-c]pyridine; compound with chloro-benzene (94532-27-1)

Guidance literature:

Multi-step reaction with 2 steps

1: various solvent(s) / Ambient temperature; in normal daylight

In various solvent(s);

DOI:10.1016/S0040-4039(01)81423-4

Reference yield:

1,3,4-tris(phenylthio)<1>benzothieno<3,2-c>pyridine (94532-23-7) + chlorobenzene (108-90-7) → 1,3,4-Tris-phenylsulfanyl-benzo[4,5]thieno[3,2-c]pyridine; compound with chloro-benzene (94532-27-1)

Guidance literature:

DOI:10.1016/S0040-4039(01)81423-4

upstream raw materials:

1,3,4-tris(phenylthio)<1>benzothieno<3,2-c>pyridine

chlorobenzene

2,3,4,5,6-pentachloropyridine

sodium thiophenolate