1-Bromo-cyclohexanecarbothioic acid S-tert-butyl ester

Base Information

• Chemical Name: 1-Bromo-cyclohexanecarbothioic acid S-tert-butyl ester
• CAS No.: 137524-50-6
• Molecular Formula: C₁₁H₁₉BrOS
• Molecular Weight: 279.241
• Mol file: 137524-50-6.mol

Synonyms:

Chemical Property of 1-Bromo-cyclohexanecarbothioic acid S-tert-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 1-Bromo-cyclohexanecarbothioic acid S-tert-butyl ester

There total 1 articles about 1-Bromo-cyclohexanecarbothioic acid S-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methylpropan-2-thiol (75-66-1) + Cyclohexanecarboxylic acid (98-89-5) → 1-Bromo-cyclohexanecarbothioic acid S-tert-butyl ester (137524-50-6)

Guidance literature:

With bromine; phosphorus tribromide; Yield given. Multistep reaction; 1.) from 100 deg C to 120 deg C, 6 h, 2.) CH₂Cl₂, RT, 16 h;

DOI:10.1080/00397919108019816

upstream raw materials:

2-methylpropan-2-thiol

Cyclohexanecarboxylic acid