N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-phenyldisulfanyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

Base Information

Chemical Name:N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-phenyldisulfanyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester
CAS No.:161959-15-5
Molecular Formula:C₃₀H₂₆N₄O₂S₆
Molecular Weight:666.958
Hs Code.:

N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-phenyldisulfanyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

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Chemical Property of N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-phenyldisulfanyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

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Technology Process of N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-phenyldisulfanyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

There total 1 articles about N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-phenyldisulfanyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13331-31-2
S-benzyldithiocarbazate

: 98892-67-2
bis(3-formyl-4-hydroxyphenyl) disulfide

: 161959-15-5
N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-phenyldisulfanyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

Guidance literature:: In methanol; for 3h; Heating;
DOI:10.1246/bcsj.68.554

Reference yield:

: 67-56-1
methanol

: bis(acetylacetonato)dioxidomolybdenum(VI)

: 161959-15-5
N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-phenyldisulfanyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

: 2Mo⁽⁶⁺⁾*4O^(2-)*C₃₀H₂₂N₄O₂S₆^(4-)=[(MoO₂)2(C₃₀H₂₂N₄O₂S₆)]

: 2Mo⁽⁶⁺⁾*4O^(2-)*C₃₀H₂₂N₄O₂S₆^(4-)*2CH₃OH=[(MoO₂)2(C₃₀H₂₂N₄O₂S₆)(CH₃OH)2]

Guidance literature:: In methanol; byproducts: acetylacetone; addn. of Mo complex to soln. of Schiff's base (shaking), filtration, refluxing (water bath, 6 h); volume reduction, cooling to 10°C (overnight), pptn., filtration,washing (MeOH), air-drying (100°C); elem. anal.;
DOI:10.1246/bcsj.68.554