Carbonylchloro(hexamethylbenzol)(trimethylphosphan)ruthenium(II)-hexafluorophosphat

Base Information

• Chemical Name: Carbonylchloro(hexamethylbenzol)(trimethylphosphan)ruthenium(II)-hexafluorophosphat
• CAS No.: 71652-19-2
• Molecular Formula: C₁₆H₂₇ClOPRu*F₆P
• Molecular Weight: 547.851
• Mol file: 71652-19-2.mol

Synonyms:

Chemical Property of Carbonylchloro(hexamethylbenzol)(trimethylphosphan)ruthenium(II)-hexafluorophosphat

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Carbonylchloro(hexamethylbenzol)(trimethylphosphan)ruthenium(II)-hexafluorophosphat

There total 1 articles about Carbonylchloro(hexamethylbenzol)(trimethylphosphan)ruthenium(II)-hexafluorophosphat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + [(η6-C6Me6)Cl(PMe3)Ru(NCCH3)]PF6 (312962-88-2) + phenylacetylene (536-74-3) → Carbonylchloro(hexamethylbenzol)(trimethylphosphan)ruthenium(II)-hexafluorophosphat (71652-19-2) + (ruthenium(hexamethylbenzene)(PMe3)(COMeCH2Ph)Cl)PF6

Guidance literature:

In methanol; dichloromethane; byproducts: C6(CH3)6; stirred under N2 for 93 h; not isolated; NMR-monitoring;

DOI:10.1021/om0004949

upstream raw materials:

methanol

[(η6-C6Me6)Cl(PMe3)Ru(NCCH3)]PF6

phenylacetylene