potassium tris(decafluorodiphenylamido) vanadium Cl

Base Information

Chemical Name:potassium tris(decafluorodiphenylamido) vanadium Cl
CAS No.:518026-95-4
Molecular Formula:C₃₆ClF₃₀N₃V*K
Molecular Weight:1169.86
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Chemical Property of potassium tris(decafluorodiphenylamido) vanadium Cl

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Technology Process of potassium tris(decafluorodiphenylamido) vanadium Cl

There total 1 articles about potassium tris(decafluorodiphenylamido) vanadium Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 1535-92-8
2,2',3,3',4,4',5,5',6,6'-decafluorodiphenylamine

: 7718-98-1
vanadium(III) chloride

: potassium hydride

: 518026-95-4
potassium tris(decafluorodiphenylamido) vanadium Cl

Guidance literature:: In tetrahydrofuran; (Ar), amine mixed with excess of KH in THF, stirred for 10 min, added toTHF soln. of metal salt, stirred at room temp. for 18 h; evapd. (vac.), washed (hexanes), extd. (toluene), filtered (Celite), evapd., crystd. (hexanes), at -35°C overnight, decanted, dried in vac.; elem. anal.;
DOI:10.1016/S0277-5387(02)01258-5