1-(α-bromo-3,4-dimethoxy-benzyl)-5,6-dimethoxy-isoquinoline

Base Information

Chemical Name:1-(α-bromo-3,4-dimethoxy-benzyl)-5,6-dimethoxy-isoquinoline
CAS No.:855647-68-6
Molecular Formula:C₂₀H₂₀BrNO₄
Molecular Weight:418.287
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(α-bromo-3,4-dimethoxy-benzyl)-5,6-dimethoxy-isoquinoline

Chemical Property:

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Technology Process of 1-(α-bromo-3,4-dimethoxy-benzyl)-5,6-dimethoxy-isoquinoline

There total 7 articles about 1-(α-bromo-3,4-dimethoxy-benzyl)-5,6-dimethoxy-isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 855617-40-2
(5,6-dimethoxy-[1]isoquinolyl)-(3,4-dimethoxy-phenyl)-ketone

: 855647-68-6
1-(α-bromo-3,4-dimethoxy-benzyl)-5,6-dimethoxy-isoquinoline

Guidance literature:: With acetic acid; zinc; und anschliessenden Behandeln des Reaktionsprodukts mit Bromwasserstoff und Essigsaeure;
DOI:10.1002/hlca.19490320114

Reference yield:

: 3213-29-4
2,3-dimethoxyphenethylamine

: 855647-68-6
1-(α-bromo-3,4-dimethoxy-benzyl)-5,6-dimethoxy-isoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: benzene

2: phosphoryl chloride; toluene

3: palladium/charcoal; decalin / 230 °C

4: zinc-dust; acetic acid / und anschliessenden Behandeln des Reaktionsprodukts mit Bromwasserstoff und Essigsaeure

With palladium on activated charcoal; acetic acid; toluene; decalin; zinc; trichlorophosphate; benzene;
DOI:10.1002/hlca.19490320114

Reference yield:

: 6831-56-7
2',3'-dimethoxyphenylacetyl chloride

: 855647-68-6
1-(α-bromo-3,4-dimethoxy-benzyl)-5,6-dimethoxy-isoquinoline

Guidance literature:: Multi-step reaction with 6 steps

1: aqueous ammonia

2: lithium alanate; diethyl ether

3: benzene

4: phosphoryl chloride; toluene

5: palladium/charcoal; decalin / 230 °C

6: zinc-dust; acetic acid / und anschliessenden Behandeln des Reaktionsprodukts mit Bromwasserstoff und Essigsaeure

With ammonium hydroxide; palladium on activated charcoal; lithium aluminium tetrahydride; diethyl ether; acetic acid; toluene; decalin; zinc; trichlorophosphate; benzene;
DOI:10.1002/hlca.19490320114