2-oxo-2,2'-(4-methyl-cyclohexylidene)-di-acetic acid

Base Information

Chemical Name:2-oxo-2,2'-(4-methyl-cyclohexylidene)-di-acetic acid
CAS No.:872276-51-2
Molecular Formula:C₁₁H₁₆O₅
Molecular Weight:228.245
Hs Code.:

Synonyms:

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Chemical Property of 2-oxo-2,2'-(4-methyl-cyclohexylidene)-di-acetic acid

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Technology Process of 2-oxo-2,2'-(4-methyl-cyclohexylidene)-di-acetic acid

There total 2 articles about 2-oxo-2,2'-(4-methyl-cyclohexylidene)-di-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85179-91-5
4-methylcyclohexane-1,1-diacetic acid

: 872276-51-2
2-oxo-2,2'-(4-methyl-cyclohexylidene)-di-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus (V)-chloride / anschliessendes Behandeln mit Brom und Erwaermen des Reaktionsgemisches mit Aethanol

2: aqueous KOH-solution / 150 °C

With potassium hydroxide; phosphorus pentachloride;
DOI:10.1039/jr9320001047

Reference yield:

: 1-methoxy-6-methyl-spiro[2.5]octane-1,2-dicarboxylic acid

: 10035-10-6,12258-64-9
hydrogen bromide

: 5433-06-7
1-carboxy-1-(4-methyl-cyclohexane) acetic acid

: 872276-51-2
2-oxo-2,2'-(4-methyl-cyclohexylidene)-di-acetic acid

Guidance literature:: (+-)-1-methoxy-6-methyl-spiro<2.5>octane-1r,2c-dicarboxylic acid of mp: 162 degree;
DOI:10.1039/jr9320001047

Reference yield:

: 872276-51-2
2-oxo-2,2'-(4-methyl-cyclohexylidene)-di-acetic acid

: 5433-06-7
1-carboxy-1-(4-methyl-cyclohexane) acetic acid

Guidance literature:: With dihydrogen peroxide; sodium carbonate; <4-methyl-1-carboxy-cyclohexyl>-acetic acid of mp: 174 degree;
DOI:10.1039/jr9320001047