4-methyl-6-((Ξ)-2,6,6-trimethyl-cyclohex-2-enylidene)-hexa-2ξ!,4ξ!-dienal; liquid substance

Base Information

Chemical Name:4-methyl-6-((Ξ)-2,6,6-trimethyl-cyclohex-2-enylidene)-hexa-2ξ!,4ξ!-dienal; liquid substance
CAS No.:875818-46-5
Molecular Formula:C₁₆H₂₂O
Molecular Weight:230.35
Hs Code.:

Synonyms:

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Chemical Property of 4-methyl-6-((Ξ)-2,6,6-trimethyl-cyclohex-2-enylidene)-hexa-2ξ!,4ξ!-dienal; liquid substance

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Technology Process of 4-methyl-6-((Ξ)-2,6,6-trimethyl-cyclohex-2-enylidene)-hexa-2ξ!,4ξ!-dienal; liquid substance

There total 11 articles about 4-methyl-6-((Ξ)-2,6,6-trimethyl-cyclohex-2-enylidene)-hexa-2ξ!,4ξ!-dienal; liquid substance which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3155-71-3
2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)-2-butenal

: 875818-46-5
4-methyl-6-((Ξ)-2,6,6-trimethyl-cyclohex-2-enylidene)-hexa-2ξ!,4ξ!-dienal; liquid substance

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂; NaHCO₃; CaO / anschliessend mit Chinolin_. Reagens 4: N-Brom-succinimid

2: liquid NH₃ / partielles Hydrieren des Reaktionsprodukts an Lindlar-Katalysator in Petrolaether in Gegenwart von Chinolin und anschliessenden Behandeln mit wss. HCl

With dichloromethane; ammonia; sodium hydrogencarbonate; calcium oxide;
DOI:10.1002/hlca.19560390130

Reference yield:

: 20013-73-4
2,6,6-trimethylcyclohex-2-en-1-one

: 875818-46-5
4-methyl-6-((Ξ)-2,6,6-trimethyl-cyclohex-2-enylidene)-hexa-2ξ!,4ξ!-dienal; liquid substance

Guidance literature:: Multi-step reaction with 6 steps

1: liquid NH₃

2: petroleum ether; quinoline / Hydrogenation_.an einem bleihaltigen Palladium-Katalysator, anschl. in Dioxan mit wss. H₂SO₄

3: H₃PO₄; water; ethanol

4: ZnCl₂; ethyl acetate

5: aqueous sodium acetate; acetic acid

6: liquid NH₃ / partielles Hydrieren des Reaktionsprodukts an Lindlar-Katalysator in Petrolaether in Gegenwart von Chinolin und anschliessenden Behandeln mit wss. HCl

With quinoline; ethanol; phosphoric acid; ammonia; water; sodium acetate; acetic acid; ethyl acetate; zinc(II) chloride; Petroleum ether;
DOI:10.1002/hlca.19560390130

Reference yield:

: 103276-11-5
2-Methyl-4-(2,6,6-trimethyl-cyclohexyliden)-buten-⁽²⁾-al-⁽¹⁾

: 875818-46-5
4-methyl-6-((Ξ)-2,6,6-trimethyl-cyclohex-2-enylidene)-hexa-2ξ!,4ξ!-dienal; liquid substance

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid

2: NaHCO₃; water; methanol

3: CH₂Cl₂; NaHCO₃; CaO / anschliessend mit Chinolin_. Reagens 4: N-Brom-succinimid

4: liquid NH₃ / partielles Hydrieren des Reaktionsprodukts an Lindlar-Katalysator in Petrolaether in Gegenwart von Chinolin und anschliessenden Behandeln mit wss. HCl

With methanol; dichloromethane; ammonia; water; sodium hydrogencarbonate; toluene-4-sulfonic acid; calcium oxide;
DOI:10.1002/hlca.19560390130