2-methyl-4-(2,6,6-trimethyl-cyclohex-2-enylidene)-crotonaldehyde diethylacetal

Base Information

Chemical Name:2-methyl-4-(2,6,6-trimethyl-cyclohex-2-enylidene)-crotonaldehyde diethylacetal
CAS No.:110146-35-5
Molecular Formula:C₁₈H₃₀O₂
Molecular Weight:278.435
Hs Code.:

Synonyms:

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Chemical Property of 2-methyl-4-(2,6,6-trimethyl-cyclohex-2-enylidene)-crotonaldehyde diethylacetal

Chemical Property:

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Technology Process of 2-methyl-4-(2,6,6-trimethyl-cyclohex-2-enylidene)-crotonaldehyde diethylacetal

There total 9 articles about 2-methyl-4-(2,6,6-trimethyl-cyclohex-2-enylidene)-crotonaldehyde diethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3155-71-3
2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)-2-butenal

: 110146-35-5
2-methyl-4-(2,6,6-trimethyl-cyclohex-2-enylidene)-crotonaldehyde diethylacetal

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂; NaHCO₃; CaO / anschliessend mit Chinolin_. Reagens 4: N-Brom-succinimid

2: ethanol; H₃PO₄

With ethanol; dichloromethane; phosphoric acid; sodium hydrogencarbonate; calcium oxide;
DOI:10.1002/hlca.19560390130

Reference yield:

: 20013-73-4
2,6,6-trimethylcyclohex-2-en-1-one

: 110146-35-5
2-methyl-4-(2,6,6-trimethyl-cyclohex-2-enylidene)-crotonaldehyde diethylacetal

Guidance literature:: Multi-step reaction with 6 steps

1: liquid NH₃

2: petroleum ether; quinoline / Hydrogenation_.an einem bleihaltigen Palladium-Katalysator, anschl. in Dioxan mit wss. H₂SO₄

3: H₃PO₄; water; ethanol

4: ZnCl₂; ethyl acetate

5: aqueous sodium acetate; acetic acid

6: ethanol; H₃PO₄

With quinoline; ethanol; phosphoric acid; ammonia; water; sodium acetate; acetic acid; ethyl acetate; zinc(II) chloride; Petroleum ether;
DOI:10.1002/hlca.19560390130

Reference yield:

: 60814-36-0
1-ethoxyethynyl-2,6,6-trimethyl-cyclohex-2-enol

: 110146-35-5
2-methyl-4-(2,6,6-trimethyl-cyclohex-2-enylidene)-crotonaldehyde diethylacetal

Guidance literature:: Multi-step reaction with 5 steps

1: petroleum ether; quinoline / Hydrogenation_.an einem bleihaltigen Palladium-Katalysator, anschl. in Dioxan mit wss. H₂SO₄

2: H₃PO₄; water; ethanol

3: ZnCl₂; ethyl acetate

4: aqueous sodium acetate; acetic acid

5: ethanol; H₃PO₄

With quinoline; ethanol; phosphoric acid; water; sodium acetate; acetic acid; ethyl acetate; zinc(II) chloride; Petroleum ether;
DOI:10.1002/hlca.19560390130