pentafluorophenyldichlorobromogermane

Base Information

• Chemical Name: pentafluorophenyldichlorobromogermane
• CAS No.: 69656-70-8
• Molecular Formula: C₆BrCl₂F₅Ge
• Molecular Weight: 390.458
• Mol file: 69656-70-8.mol

Synonyms:

Chemical Property of pentafluorophenyldichlorobromogermane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of pentafluorophenyldichlorobromogermane

There total 2 articles about pentafluorophenyldichlorobromogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

Hexafluorobenzene (392-56-3) + 2,3,4,5,6-pentafluorophenylmagnesium bromide (879-05-0) + germaniumtetrachloride (10038-98-9) → (pentafluorophenyl)trichlorogermane (69656-69-5) + (pentafluoro phenyl) tribromo germane (35369-95-0) + pentafluorophenylchlorodibromogermane (69656-71-9) + pentafluorophenyldichlorobromogermane (69656-70-8)

Guidance literature:

In diethyl ether; benzene; byproducts: (C6F5)2GeBr2, (C6F5)3GeBr; GeCl4 in benzene added to etheric soln. of C6F5MgBr; driving off ether and replacing by more C6F6; refluxing for 10 h;

Reference yield: 51.0%

Hexafluorobenzene (392-56-3) + 2,3,4,5,6-pentafluorophenylmagnesium bromide (879-05-0) + germaniumtetrachloride (10038-98-9) → (pentafluoro phenyl) tribromo germane (35369-95-0) + bis(pentafluorophenyl)germanium dibromide (10177-65-8) + pentafluorophenylchlorodibromogermane (69656-71-9) + pentafluorophenyldichlorobromogermane (69656-70-8) + tris(pentafluorophenyl)germanium bromide (10360-39-1)

Guidance literature:

In diethyl ether; benzene; GeCl4 in benzene added to etheric soln. of C6F5MgBr; driving off ether and replacing by more C6F6; refluxing for 10 h;

upstream raw materials:

Hexafluorobenzene

2,3,4,5,6-pentafluorophenylmagnesium bromide

germaniumtetrachloride