(2-[bis(trimethylsilyl)methyl]-4-(ethoxycarbonyl)-5-[trans-2-(ethoxycarbonyl)-3-(triphenylphosphonio)propenylidyl]-2H-1,2-azaphosphole-κP)pentacarbonyltungsten(0)

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Chemical Name:(2-[bis(trimethylsilyl)methyl]-4-(ethoxycarbonyl)-5-[trans-2-(ethoxycarbonyl)-3-(triphenylphosphonio)propenylidyl]-2H-1,2-azaphosphole-κP)pentacarbonyltungsten(0)
CAS No.:441794-07-6
Molecular Formula:C₄₂H₄₇NO₉P₂Si₂W
Molecular Weight:1011.81
Hs Code.:

(2-[bis(trimethylsilyl)methyl]-4-(ethoxycarbonyl)-5-[trans-2-(ethoxycarbonyl)-3-(triphenylphosphonio)propenylidyl]-2H-1,2-azaphosphole-κP)pentacarbonyltungsten(0)

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Chemical Property of (2-[bis(trimethylsilyl)methyl]-4-(ethoxycarbonyl)-5-[trans-2-(ethoxycarbonyl)-3-(triphenylphosphonio)propenylidyl]-2H-1,2-azaphosphole-κP)pentacarbonyltungsten(0)

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Technology Process of (2-[bis(trimethylsilyl)methyl]-4-(ethoxycarbonyl)-5-[trans-2-(ethoxycarbonyl)-3-(triphenylphosphonio)propenylidyl]-2H-1,2-azaphosphole-κP)pentacarbonyltungsten(0)

There total 1 articles about (2-[bis(trimethylsilyl)methyl]-4-(ethoxycarbonyl)-5-[trans-2-(ethoxycarbonyl)-3-(triphenylphosphonio)propenylidyl]-2H-1,2-azaphosphole-κP)pentacarbonyltungsten(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 171625-87-9
pentacarbonyl[2-(bis(trimethylsilyl)methyl)-3-phenyl-2H-azaphosphirene-κP]tungsten(0)

: 16640-68-9
cyanomethylene triphenylphosphorane

: 623-47-2
propynoic acid ethyl ester

: 441794-06-5
(2-[bis(trimethylsilyl)methyl]-4-(ethoxycarbonyl)-5-[(triphenylphosphonio)methylidyl]-2H-1,2-azaphosphole-κP)pentacarbonyltungsten(0)

: 441794-07-6
(2-[bis(trimethylsilyl)methyl]-4-(ethoxycarbonyl)-5-[trans-2-(ethoxycarbonyl)-3-(triphenylphosphonio)propenylidyl]-2H-1,2-azaphosphole-κP)pentacarbonyltungsten(0)

Guidance literature:: In toluene; byproducts: C6H5CN; soln. of starting materials in toluene stirred at 75°C for 2 h under N2; evapn. of volatile components in vacuo, chromy. (SiO2, -10°C, n-pentane/diethyl ether 70:30); elem. anal.;
DOI:10.1002/1099-0682(200203)2002:4<957::AID-EJIC957>3.0.CO;2-2