Stannane, (4-methyl-1,2-phenylene)bis[trimethyl-

Base Information

Chemical Name:Stannane, (4-methyl-1,2-phenylene)bis[trimethyl-
CAS No.:14275-63-9
Molecular Formula:C13H24Sn2
Molecular Weight:417.754
Hs Code.:
DSSTox Substance ID:DTXSID30445248
Wikidata:Q82263605

Synonyms:Stannane, (4-methyl-1,2-phenylene)bis[trimethyl-;14275-63-9;DTXSID30445248

Suppliers and Price of Stannane, (4-methyl-1,2-phenylene)bis[trimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Stannane, (4-methyl-1,2-phenylene)bis[trimethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:417.99161
Heavy Atom Count:15
Complexity:210

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)[Sn](C)(C)C)[Sn](C)(C)C

Technology Process of Stannane, (4-methyl-1,2-phenylene)bis[trimethyl-

There total 5 articles about Stannane, (4-methyl-1,2-phenylene)bis[trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 436850-39-4
2-bromo-4-methyl-1-(trimethylstannyl)benzene

: 1529-47-1
chlorotrimethylgermane

: 14275-63-9
4-methyl-1,2-bis(trimethylstannyl)benzene

: 436850-41-8
4-methyl-1,2-bis(trimethylgermyl)benzene

: 436850-40-7
4-methyl-2-trimethylgermyl-1-(trimethylstannyl)benzene

Guidance literature:: With Mg; In tetrahydrofuran; using high-vac. techniques; mixt. of C6H3(Br)(SnMe3)(Me), Mg and THF stirred for 1 - 25 ds; quenched with Me3GeCl; Et2O added; org. fraction sepd.; aq. fraction extd. (Et2O); org. fractions combined; dried (MgSO4); filtered; evapd. to dryness; elem. anal.;
DOI:10.1021/om011083a

Reference yield: 94.0%

: 436850-39-4
2-bromo-4-methyl-1-(trimethylstannyl)benzene

: 7789-20-0
water-d2

: 14275-63-9
4-methyl-1,2-bis(trimethylstannyl)benzene

: 436850-55-4
2-deuterio-4-methyl-1-(trimethylstannyl)benzene

Guidance literature:: With Mg; In tetrahydrofuran; using high-vac. techniques; mixt. of C6H3(Br)(SnMe3)(Me), Mg and THF stirred for 1 - 25 ds; deuteriolyzed (D2O); Et2O added; org. fraction sepd.; org. fraction dried (MgSO4); analyzed by GCMS;
DOI:10.1021/om011083a

Reference yield: 24.0%

: 661-69-8
hexamethyldistannane

: 3-methyl-6-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 14275-63-9
4-methyl-1,2-bis(trimethylstannyl)benzene

: 873196-55-5
(CH₃C₆H₃(Sn(CH₃)3))2

: 873196-54-4
(CH₃C₆H₃(Sn(CH₃)3))2

: 873196-53-3
(CH₃C₆H₃(Sn(CH₃)3))2

Guidance literature:: With 18-crown-6 ether; ethriol phosphite; In tetrahydrofuran; Si compd.:Sn compd.=3:1 molar ratio, with KF at 20°C for 5 h;
DOI:10.1039/b511773a