MeO⁽¹³⁾C(O)Ir(Me)(I)(CO)(PPh₃)2

Base Information

• Chemical Name: MeO⁽¹³⁾C(O)Ir(Me)(I)(CO)(PPh₃)2
• CAS No.: 118626-13-4
• Molecular Formula: C₄₀H₃₆IIrO₃P₂
• Molecular Weight: 946.785

Synonyms:

Chemical Property of MeO⁽¹³⁾C(O)Ir(Me)(I)(CO)(PPh₃)2

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of MeO⁽¹³⁾C(O)Ir(Me)(I)(CO)(PPh₃)2

There total 3 articles about MeO⁽¹³⁾C(O)Ir(Me)(I)(CO)(PPh₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(MeO)Ir(Me)(I)(CO)(PPh3)2 (107799-54-2) + carbon monoxide (201230-82-2) → MeOC(O)Ir(Me)(I)(CO)(PPh3)2 (118626-13-4)

Guidance literature:

In acetonitrile; suspn. of complex in a pressure bottle flushed several times, charged with CO (60 psi), stirred (room temp., 2 d); solvent removed in vac., benzene added, stirred (5 min), evapd.;

DOI:10.1021/om00105a034

Reference yield:

(MeO)Ir(Me)(I)(CO)(PPh3)2 (107799-54-2) + [13C]Carbon monoxide (1641-69-6) → MeO(13)C(O)Ir(Me)(I)(CO)(PPh3)2 (118626-13-4)

Guidance literature:

In acetonitrile; suspn. of complex in a pressure bottle flushed, charged with (13)CO (60 si), stirred 14 h, room temp.); solvent removed in vac., benzene added, soln. stirred (5 min), solvent removed;

DOI:10.1021/om00105a034

Reference yield:

MeOC(O)Ir(Me)(I)(PPh3)2 (118515-37-0) + carbon monoxide (201230-82-2) → MeOC(O)Ir(Me)(I)(CO)(PPh3)2 (118626-13-4)

Guidance literature:

In acetonitrile; CO passed over soln. of complex in a Schlenk flask (N2) (8 h, 45°C);

DOI:10.1021/om00105a034

upstream raw materials:

(MeO)Ir(Me)(I)(CO)(PPh₃)2

carbon monoxide

MeOC(O)Ir(Me)(I)(PPh₃)2

[13C]Carbon monoxide

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