(2-Aminoethyl)butylphenylarsine

Base Information

Chemical Name:(2-Aminoethyl)butylphenylarsine
CAS No.:97067-29-3
Molecular Formula:C₁₂H₂₀AsN
Molecular Weight:253.219
Hs Code.:

Synonyms:

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Chemical Property of (2-Aminoethyl)butylphenylarsine

Chemical Property:

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Technology Process of (2-Aminoethyl)butylphenylarsine

There total 2 articles about (2-Aminoethyl)butylphenylarsine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 829-83-4
diphenylarsane

: 97067-29-3,97101-68-3,97101-69-4
(2-Aminoethyl)butylphenylarsine

Guidance literature:: Multi-step reaction with 2 steps

1: 1)BuLi / 1)THF,hexane, 1 h,room temp., 2)50 deg C,1 h, reflux 6h, room temp. 12h;

2: 1) Na / 1) NH₃(l) 3h;

With n-butyllithium; sodium;
DOI:10.1246/bcsj.58.258

Reference yield:

: 109-65-9
1-bromo-butane

: 31699-82-8
(2-Aminoethyl)diphenylarsine

: 97067-29-3,97101-68-3,97101-69-4
(2-Aminoethyl)butylphenylarsine

Guidance literature:: With sodium; Yield given. Multistep reaction; 1) NH₃(l) 3h;;
DOI:10.1246/bcsj.58.258

Reference yield:

: ammonium hexafluorophosphate

: (-)-di-μ-chloro-bis[(S)-N,N-dimethyl(α-methylbenzyl)aminate-2-C,N]dipalladium(II)

: 97067-29-3,97101-68-3,97101-69-4
(2-Aminoethyl)butylphenylarsine

: [(S)-N,N-dimethyl-α-methylbenzylamine-2C,N][(S)-(2-aminoethyl)butylphenylarsine]palladium(II) chloride

: [(S)-N,N-dimethyl-α-methylbenzylamine-2C,N][(R)-(2-aminoethyl)butylphenylarsine]palladium(II) hexafluorophosphate

Guidance literature:: In water; benzene; under N2, to soln. of Pd complex in C6H6 added soln. of ligand in C6H6,stirred for 2 h at room temp., (i), mother liquor evapd., mixed with boiling water, concd., NH4PF6 added, (ii); (i): hexane added with stirring, kept for 1 h at room temp., cooled at 0°C for 1 h, crystals collected, washed with hexane, recrystd. (MeOH-C6H6); (ii): ppt. dissolved in MeOH, slowly evapd at room temp, recrystd. (MeOH-C6H6); elem. anal.;
DOI:10.1246/bcsj.58.258