((HSC₆H₄NHCOCH₂NCH₂COOC₂H₄)2NCH₂COO)Yb

Base Information

Chemical Name:((HSC₆H₄NHCOCH₂NCH₂COOC₂H₄)2NCH₂COO)Yb
CAS No.:1261477-35-3
Molecular Formula:C₂₆H₃₀N₅O₈S₂Yb
Molecular Weight:777.725
Hs Code.:

((HSC<sub>6</sub>H<sub>4</sub>NHCOCH<sub>2</sub>NCH<sub>2</sub>COOC<sub>2</sub>H<sub>4</sub>)2NCH<sub>2</sub>COO)Yb

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Chemical Property of ((HSC₆H₄NHCOCH₂NCH₂COOC₂H₄)2NCH₂COO)Yb

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Technology Process of ((HSC₆H₄NHCOCH₂NCH₂COOC₂H₄)2NCH₂COO)Yb

There total 2 articles about ((HSC₆H₄NHCOCH₂NCH₂COOC₂H₄)2NCH₂COO)Yb which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 601473-66-9
N,N′′-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N′,N′′-triacetic acid

: 10035-01-5
ytterbium(III) chloride hexahydrate

: 1261477-35-3
((HSC₆H₄NHCOCH₂NCH₂COOC₂H₄)2NCH₂COO)Yb

Guidance literature:: In methanol; triacetic acid-compound was added to a soln. of salt in degassed methanol and sonicated; CH3CN was added, ppt. was filtered under N2, washed with CH3CN and diethyl ether, dried in vac.;
DOI:10.1021/ja109157g

Reference yield: 27.0%

: 10035-01-5
ytterbium(III) chloride hexahydrate

: tripotassium N,N'-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N',N''-triacetate

: 1261477-35-3
((HSC₆H₄NHCOCH₂NCH₂COOC₂H₄)2NCH₂COO)Yb

Guidance literature:: In water; Ln-salt was addedm to an aq. soln. of triacetate-compound; ppt. was suction filtered, washed with acetone (twice) and diethyl ether, dried under vac.;
DOI:10.1021/ja109157g