1,3-Benzenediacetic acid, 2-methoxy-, diethyl ester

Base Information

Chemical Name:1,3-Benzenediacetic acid, 2-methoxy-, diethyl ester
CAS No.:144587-92-8
Molecular Formula:C15H20O5
Molecular Weight:280.321
Hs Code.:

Synonyms:

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Chemical Property of 1,3-Benzenediacetic acid, 2-methoxy-, diethyl ester

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Technology Process of 1,3-Benzenediacetic acid, 2-methoxy-, diethyl ester

There total 4 articles about 1,3-Benzenediacetic acid, 2-methoxy-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 64-17-5
ethanol

: 144316-88-1
2,6-bis(carboxymethyl)anisole

: 144587-92-8
(3-Ethoxycarbonylmethyl-2-methoxy-phenyl)-acetic acid ethyl ester

Guidance literature:: With toluene-4-sulfonic acid;
DOI:10.1021/jo00051a010

Reference yield:

: 1004-66-6
2-methoxy-1,3-dimethylbenzene

: 144587-92-8
(3-Ethoxycarbonylmethyl-2-methoxy-phenyl)-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / N,N'-dibromo-5,5-dimethylhydantoin, benzoyl peroxide / CCl₄ / 2 h / Heating; Irradiation

2: 95 percent / hexadecyldimethylethylammonium bromide / benzene; H₂O / 5 h / Heating

3: 91 percent / 7percent aq. NaOH / Heating

4: 93 percent / p-toluenesulfonic acid

With sodium hydroxide; Perbenzoic acid; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; hexadecyldimethylethylammonium bromide; toluene-4-sulfonic acid; In tetrachloromethane; water; benzene;
DOI:10.1021/jo00051a010

Reference yield:

: 30787-74-7
2,6-bis(bromomethyl)anisole

: 144587-92-8
(3-Ethoxycarbonylmethyl-2-methoxy-phenyl)-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / hexadecyldimethylethylammonium bromide / benzene; H₂O / 5 h / Heating

2: 91 percent / 7percent aq. NaOH / Heating

3: 93 percent / p-toluenesulfonic acid

With sodium hydroxide; hexadecyldimethylethylammonium bromide; toluene-4-sulfonic acid; In water; benzene;
DOI:10.1021/jo00051a010