2-(Naphthalen-2-yloxy)-1-phenylethanone

Base Information

• Chemical Name: 2-(Naphthalen-2-yloxy)-1-phenylethanone
• CAS No.: 14538-46-6
• Molecular Formula: C18H14O2
• Molecular Weight: 262.308
• DSSTox Substance ID: DTXSID70355216
• Nikkaji Number: J1.369.095B
• Wikidata: Q82133969
• ChEMBL ID: CHEMBL1725263

Synonyms:2-(naphthalen-2-yloxy)-1-phenylethanone;14538-46-6;HMS2794P06;Ethanone, 2-(2-naphthalenyloxy)-1-phenyl-;CBMicro_000008;Oprea1_107953;MLS001178580;SCHEMBL1312768;CHEMBL1725263;DTXSID70355216;SMSF0005505;2-(2-naphthyloxy)-1-phenylethanone;AKOS008909143;CB01160;SMR000475985;BIM-0000086.P001;2-(naphthalen-2-yloxy)-1-phenylethan-1-one;SR-01000204040;SR-01000204040-1

Chemical Property of 2-(Naphthalen-2-yloxy)-1-phenylethanone

Chemical Property:

• XLogP3: 4.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 262.099379685
• Heavy Atom Count: 20
• Complexity: 319

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)COC2=CC3=CC=CC=C3C=C2

Technology Process of 2-(Naphthalen-2-yloxy)-1-phenylethanone

There total 6 articles about 2-(Naphthalen-2-yloxy)-1-phenylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

α-bromoacetophenone (70-11-1) + β-naphthol (135-19-3) → 2-(naphthalene-2-yloxy)-1-phenylethanone (14538-46-6)

Guidance literature:

With potassium hydroxide; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; at 60 ℃; for 2h;

DOI:10.1080/00304940409355387

Reference yield: 80.4%

α-bromoacetophenone (70-11-1) + β-naphthol (135-19-3) → 2-(naphthalene-2-yloxy)-1-phenylethanone (14538-46-6) + 3-phenylnaphtho[2,3-b]furan

Guidance literature:

With aluminum oxide; potassium carbonate; for 0.0833333h; Microwave irradiation;

DOI:10.1080/00397910902883702

Reference yield: 45.0%

2-diazo-acetophenone (3282-32-4) + β-naphthol (135-19-3) → 2-(naphthalene-2-yloxy)-1-phenylethanone (14538-46-6)

Guidance literature:

In(OSO₂CF₃)3; at 20 ℃;

DOI:10.1016/S0040-4039(02)00489-6

upstream raw materials:

sodium 2-naphtholate

α-bromoacetophenone

β-naphthol

2-diazo-acetophenone

Downstream raw materials:

(S)-2-(naphthalen-2-yloxy)-1-phenylethanol

phenyl-1 naphto<2,1-b>furanne

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