(But-3-yn-2-yl)(trimethyl)silane

Base Information

Chemical Name:(But-3-yn-2-yl)(trimethyl)silane
CAS No.:14583-73-4
Molecular Formula:C7H14Si
Molecular Weight:126.274
Hs Code.:
DSSTox Substance ID:DTXSID40510931
Mol file:14583-73-4.mol

Synonyms:(But-3-yn-2-yl)(trimethyl)silane;14583-73-4;DTXSID40510931

Suppliers and Price of (But-3-yn-2-yl)(trimethyl)silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (But-3-yn-2-yl)(trimethyl)silane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:126.086476981
Heavy Atom Count:8
Complexity:110

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C#C)[Si](C)(C)C

Technology Process of (But-3-yn-2-yl)(trimethyl)silane

There total 1 articles about (But-3-yn-2-yl)(trimethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85332-18-9
but-1-yne-1,3-diylbis(trimethylsilane)

: 107-46-0
Hexamethyldisiloxane

: 14583-73-4
Trimethyl-(1-methylpropin-⁽²⁾-yl)-silan

Guidance literature:: With potassium cyanide; silver nitrate; Yield given. Multistep reaction. Title compound not separated from byproducts; 1.) EtOH, H₂O, 0-5 deg C, 15 min, 2.) EtOH, H₂O, 20 deg C, 2 h;

Reference yield: 87.0%

: 14583-73-4
Trimethyl-(1-methylpropin-⁽²⁾-yl)-silan

: 2043-61-0
cyclohexanecarbaldehyde

: 215546-28-4
1-Cyclohexyl-4-trimethylsilanyl-pent-2-yn-1-ol

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; 1.) 0 deg C, 75 min, 2.) 30 min;

Reference yield:

: 14583-73-4
Trimethyl-(1-methylpropin-⁽²⁾-yl)-silan

: Acetic acid (Z)-(1R,4R)-1-cyclohexyl-4-trimethylsilanyl-pent-2-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / n-BuLi / diethyl ether; hexane / 1.) 0 deg C, 75 min, 2.) 30 min

2: 16 percent / H₂, quinoline / 5percent Pd/BaSO₄ / methanol / 3.5 h

3: 84 percent / DMAP, Et₃N / diethyl ether / 20 °C

With quinoline; dmap; n-butyllithium; hydrogen; triethylamine; Pd-BaSO₄; In methanol; diethyl ether; hexane;