3-(Benzyloxy)-4-nitrobenzoyl chloride

Base Information

Chemical Name:3-(Benzyloxy)-4-nitrobenzoyl chloride
CAS No.:14617-30-2
Molecular Formula:C14H10ClNO4
Molecular Weight:291.691
Hs Code.:
DSSTox Substance ID:DTXSID501273025
Mol file:14617-30-2.mol

Synonyms:14617-30-2;3-(benzyloxy)-4-nitrobenzoyl chloride;SCHEMBL9274861;DTXSID501273025;4-Nitro-3-(phenylmethoxy)benzoyl chloride;EN300-27147527

Suppliers and Price of 3-(Benzyloxy)-4-nitrobenzoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(Benzyloxy)-4-nitrobenzoyl chloride

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:291.0298355
Heavy Atom Count:20
Complexity:352

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC2=C(C=CC(=C2)C(=O)Cl)[N+](=O)[O-]

Technology Process of 3-(Benzyloxy)-4-nitrobenzoyl chloride

There total 6 articles about 3-(Benzyloxy)-4-nitrobenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 14617-29-9
4-nitro-3-phenylmethoxybenzoic acid

: 14617-30-2
3-(benzyloxy)-4-nitrobenzoyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 5 ℃; for 4h;

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 14617-30-2
3-(benzyloxy)-4-nitrobenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

2: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 0 °C-20 °C / Inert atmosphere

With oxalyl dichloride; sodium hydride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm501440q

Reference yield:

: 403-21-4
3-fluoro-4-nitrobenzoic acid

: 14617-30-2
3-(benzyloxy)-4-nitrobenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

2: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 0 °C-20 °C / Inert atmosphere

With oxalyl dichloride; sodium hydride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm501440q