3-Methyl-1-(4-methylphenyl)but-2-en-1-one

Base Information

Chemical Name:3-Methyl-1-(4-methylphenyl)but-2-en-1-one
CAS No.:14618-89-4
Molecular Formula:C12H14O
Molecular Weight:174.243
Hs Code.:
European Community (EC) Number:683-549-4
DSSTox Substance ID:DTXSID60392079
Nikkaji Number:J2.140.375J
Mol file:14618-89-4.mol

Synonyms:3-methyl-1-(4-methylphenyl)but-2-en-1-one;14618-89-4;SCHEMBL8844390;DTXSID60392079;Isobutenyl(4-methylphenyl) ketone;AKOS017515112;3-Methyl-1-(p-tolyl)but-2-en-1-one;3-methyl-1-(4-methylphenyl)-2-buten-1-one

Suppliers and Price of 3-Methyl-1-(4-methylphenyl)but-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-Methyl-1-(4-methylphenyl)but-2-en-1-one

Chemical Property:

PSA：17.07000
LogP:3.14390
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:174.104465066
Heavy Atom Count:13
Complexity:203

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)C=C(C)C

Technology Process of 3-Methyl-1-(4-methylphenyl)but-2-en-1-one

There total 15 articles about 3-Methyl-1-(4-methylphenyl)but-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3-methyl-1-(p-tolyl)but-3-en-1-one

: 14618-89-4
4-methyl-β,β-dimethylacrylophenone

Guidance literature:: With 5,5’-bis(diphenylphosphino)-2,2,2’,2’-tetrafluoro-4,4’-bi-1,3-benzodioxole; methanol; carbon monoxide; palladium diacetate; toluene-4-sulfonic acid; In toluene; at 40 ℃; for 24h; under 22502.3 Torr; Autoclave;
DOI:10.1002/anie.202105977

Reference yield: 84.0%

: 820-71-3
methallyl acetate

: 201230-82-2
carbon monoxide

: 5720-05-8
4-methylphenylboronic acid

: 14618-89-4
4-methyl-β,β-dimethylacrylophenone

Guidance literature:: With potassium phosphate tribasic trihydrate; palladium diacetate; tricyclohexylphosphine; In 1,4-dioxane; water; toluene; at 120 ℃; for 12h; under 3750.38 Torr; chemoselective reaction; Autoclave;
DOI:10.1039/c5cc02094h

Reference yield: 20.0%

: 1360924-11-3
allyl 2-oxo-2-(p-tolyl)acetate

: 1360924-17-9
2-methylallyl 2-oxo-2-phenylacetate

: 35660-91-4,35845-66-0,495-41-0
(E)-1-phenyl-2-buten-1-one

: 5650-07-7
3-methyl-1-phenyl-but-2-en-1-one

: 3837-95-4
(E)-1-(4-methylphenyl)-2-buten-1-one

: 14618-89-4
4-methyl-β,β-dimethylacrylophenone

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; Tri(p-tolyl)phosphine; In 1,3,5-trimethyl-benzene; at 150 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201102584