[MeN(CH₂CHPhO)(C₆H₄-o-O)]2Ti

Base Information

• Chemical Name: [MeN(CH₂CHPhO)(C₆H₄-o-O)]2Ti
• CAS No.: 1004984-55-7
• Molecular Formula: C₃₀H₃₀N₂O₄Ti
• Molecular Weight: 530.459
• Mol file: 1004984-55-7.mol

Synonyms:

Chemical Property of [MeN(CH₂CHPhO)(C₆H₄-o-O)]2Ti

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of [MeN(CH₂CHPhO)(C₆H₄-o-O)]2Ti

There total 1 articles about [MeN(CH₂CHPhO)(C₆H₄-o-O)]2Ti which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

titanium(IV) isopropylate (546-68-9) + MeN(CHPhCH2OH)(C6H4-o-OH) (1004984-50-2) + MeN(CH2CHPhOH)(C6H4-o-OH) (1004984-51-3) → [MeN(CHPhCH2O)(C6H4-o-O)]2Ti (1004984-54-6) + [MeN(CH2CHPhO)(C6H4-o-O)]2Ti (1004984-55-7)

Guidance literature:

In toluene; under Ar atm. Ti(i-OPr)4 was added dropwise to soln. mixt. ligand in toluene and refluxed for 5 h; solvent was evapd. in vacuo, residue was crystd. from CH2Cl2-heptane (1:1), isomers were not separated; elem. anal.;

DOI:10.1016/j.jorganchem.2007.10.020

upstream raw materials:

titanium(IV) isopropylate

MeN(CHPhCH₂OH)(C₆H₄-o-OH)

MeN(CH₂CHPhOH)(C₆H₄-o-OH)