(E)-4-oxo-4-(2,4,5-trichloroanilino)-2-butenoic acid

Base Information

Chemical Name:(E)-4-oxo-4-(2,4,5-trichloroanilino)-2-butenoic acid
CAS No.:31460-72-7
Molecular Formula:C10H6 Cl3 N O3
Molecular Weight:294.5185
Hs Code.:
NSC Number:137042
Mol file:31460-72-7.mol

Synonyms:31460-72-7;(E)-4-oxo-4-(2,4,5-trichloroanilino)-2-butenoic acid;(E)-4-oxo-4-(2,4,5-trichloroanilino)but-2-enoic acid;Maleanilic acid,2',4',5'-trichloro- (6CI,8CI);(E)-4-oxo-4-((2,4,5-trichlorophenyl)amino)but-2-enoic acid;NSC137042;MFCD02603163;STK053107;AKOS000489408;NSC-137042;1081849-32-2;CS-0363124;A820953;SR-01000234979;SR-01000234979-1;(2E)-4-oxo-4-[(2,4,5-trichlorophenyl)amino]but-2-enoic acid;(E)-4-oxidanylidene-4-[[2,4,5-tris(chloranyl)phenyl]amino]but-2-enoic acid

Suppliers and Price of (E)-4-oxo-4-(2,4,5-trichloroanilino)-2-butenoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of (E)-4-oxo-4-(2,4,5-trichloroanilino)-2-butenoic acid

Chemical Property:

Vapor Pressure:8.85E-11mmHg at 25°C
Boiling Point:499.1°C at 760 mmHg
Flash Point:255.6°C
Density:1.639g/cm³
XLogP3:2.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:292.941326
Heavy Atom Count:17
Complexity:335

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C(=CC(=C1Cl)Cl)Cl)NC(=O)C=CC(=O)O
Isomeric SMILES:C1=C(C(=CC(=C1Cl)Cl)Cl)NC(=O)/C=C/C(=O)O

Technology Process of (E)-4-oxo-4-(2,4,5-trichloroanilino)-2-butenoic acid

There total 1 articles about (E)-4-oxo-4-(2,4,5-trichloroanilino)-2-butenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 108-31-6
maleic anhydride

: 636-30-6
2,4,5-trichloroaniline

: 31460-72-7
(Z)-3-(2,4,5-Trichloro-phenylcarbamoyl)-acrylic acid

Guidance literature:: In diethyl ether; at 20 ℃;

Reference yield: 48.0%

: 31460-72-7
(Z)-3-(2,4,5-Trichloro-phenylcarbamoyl)-acrylic acid

: 67-56-1
methanol

: 915711-49-8
(Z)-3-(2,4,5-Trichloro-phenylcarbamoyl)-acrylic acid methyl ester

Guidance literature:: With phosphorus pentaoxide; Heating;

Reference yield:

: 31460-72-7
(Z)-3-(2,4,5-Trichloro-phenylcarbamoyl)-acrylic acid

: 2-(3-oxo-3,4-dihydro-2H-benzo[1,4]thiazin-2-yl)-N-(2,4,5-trichloro-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / phosphorus pentoxide / Heating

2: 66 percent / aniline / ethanol / Heating

3: 63 percent / dimethylformamide / Heating

With phosphorus pentaoxide; aniline; In ethanol; N,N-dimethyl-formamide;